The application provides a monovalent
ionic liquid fiber membrane, a preparation method and application in
recovery of
palladium, and belongs to the technical field of adsorbing materials, and comprises the following steps: mixing
dichloromethane and
acetic acid to obtain a first solution; dissolving
cellulose acetate and
ionic liquid in the first solution to obtain a second solution; the
ionic liquid is any one of an alkenyl
imidazole salt, a
quaternary ammonium salt containing an alkenyl group, a
quaternary phosphonium salt containing an alkenyl group, a
pyridine salt containing an alkenyl group or a
morpholine salt containing an alkenyl group; N,N'-
methylene bisacrylamide and
benzoyl peroxide are added into the second solution, heated, stirred and warmed to obtain a third solution, and the third solution is subjected to high-pressure
electrospinning to obtain the monovalent ionic liquid
fiber membrane; or the second solution is subjected to high-pressure
electrospinning and then
irradiation to obtain the monovalent ionic liquid
fiber membrane. The monovalent ionic liquid fiber membrane prepared by the application can realize rapid adsorption and easy regeneration and
desorption, and can efficiently and selectively adsorb and recover
palladium from a complex acidic solution.