The application discloses a preparation method of a high-entropy MXene composite diaphragm
coating, which comprises the following steps: in the first step, 2g of HE-MAX phase
raw material powder is gradually added into a reaction container containing an HF solution to perform a chemical
etching reaction, and meanwhile, the sample is magnetically stirred at 55 DEG C for 72 to 96h; in the second step, the obtained HE-MXene suspension is placed into a centrifugal tube, and the precipitate is collected by high-speed
centrifugation, and the deionized water and
anhydrous ethanol are repeatedly cleaned until the solution is close to neutral; in the third step, the obtained precipitate is vacuum dried at 60 DEG C for 12h to obtain HE-MXene
nanosheet powder; in the fourth step, the HE-MXene and two-dimensional layered material
powder are weighed according to a weight ratio of 7:3, and after
grinding, they are dissolved into deionized water and stirred to prepare an HE-MXene suspension; in the fifth step, after magnetic stirring is used until the mixed state is reached, vacuum
filtration is performed; in the sixth step, the obtained HE-MXene / two-dimensional layered material@PP is placed in a vacuum environment and dried at 40 DEG C for 6h, and finally, the modified diaphragm is
cut into a disc with a
diameter of 18mm.