Method of marking composition for oral administration
A marking method and composition technology, applied in the field of identification marking, can solve the problems of adhesion, insufficient information of the marking sheet, smudged printing on the tablet, etc., and achieve the effect of high stability
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Embodiment 1
[0095] (Example 1) tablet
[0096] Mix 80g of lactose, 20g of cornstarch, 0.5g of magnesium stearate, 1g of titanium oxide or 0.2g of yellow ferric oxide, and compress it with a tablet machine or an autograph material tester to obtain tablets.
[0097] Using a laser device (Photonics Industries International, Inc.) shown in Table 1, 100 tablets spread over a 10 cm x 10 cm disk were irradiated with laser light under the conditions shown in Table 1. The result was tablets with excellent visible markings when containing titanium oxide or yellow ferric oxide. On the other hand, its surface is not etched.
Embodiment 2
[0098] (Example 2) tablet
[0099] Mix 80g of lactose, 20g of cornstarch, 0.5g of magnesium stearate, 0.01g of titanium oxide or 0.006g of yellow ferric oxide, and compress it with a tablet machine or an automatic plotter material testing machine to obtain tablets. The above samples were marked using the laser device and irradiation conditions shown in Table 1. As a result, discoloration was observed, resulting in a poorly visible mark.
[0100] [Table 1]
[0101] laser name
[0102] Manufacturer: Photonics Industries International, Inc.
Embodiment 3
[0108] (embodiment 3) soft capsules
[0109] A soft capsule with a gelatin coating layer was prepared by a rotational molding method, and the gelatin coating layer contained 20 parts by mass of concentrated glycerin, 10 parts by mass of D-sorbitol and 1 part by mass of titanium oxide relative to 100 parts by mass of gelatin. Adopt the laser device shown in Table 1 and the irradiation condition, mark text E268 to this soft capsule (white) along the major diameter axis direction of soft capsule. As a result, a gray soft capsule with an excellent visibility mark was obtained. On the other hand, an attempt to mark the same characters with a carbon dioxide laser (ML-G9300 series manufactured by KEYENCE; 1060nm) was able to form white characters on the surface of the soft capsule through foaming, but the visibility of the white characters on a white base was poor.
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