Process for abstracting solanesol in waste of white potato haulm auxiliary by microwave
A potato stem and leaf, microwave-assisted technology is applied in the separation/purification of hydroxyl compounds, pharmaceutical formulations, plant raw materials, etc., to achieve the effects of promoting economic development, controllable reaction conditions, and reducing consumption
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Embodiment 1
[0028] A method for microwave-assisted extraction of solanesol in potato stem and leaf waste of the present invention comprises the following steps:
[0029] 1) Get potato stems and leaves, pulverize, cross 40 mesh sieves, add 95% ethanol and stir evenly, the weight ratio of described potato stems and leaves and 95% ethanol is 1: 1, put the mixed solution of potato stems and leaves and 95% ethanol In the microwave drying equipment, the microwave frequency is 2450MHz, the power is 1100W, the control temperature is 35°C, and the microwave is irradiated for 15 minutes under the condition of vacuum degree of 0.08MPa to obtain substance A;
[0030] 2) Add 95% ethanol to substance A, the weight ratio of substance A to 95% ethanol is 1:8, under the condition that the microwave frequency is 2450MHz, the power is 1200W, the temperature is 55°C, and the stirring speed is 80 rpm under microwave-assisted reflux extraction for 50 minutes, then suction-filtered under the condition of 0.08MP...
Embodiment 2
[0034] A method for microwave-assisted extraction of solanesol in potato stem and leaf waste of the present invention comprises the following steps:
[0035] 1) Get potato stems and leaves, pulverize, cross 40 mesh sieves, add 95% ethanol and stir evenly, the weight ratio of described potato stems and leaves and 95% ethanol is 1: 1, put the mixed solution of potato stems and leaves and 95% ethanol In the microwave drying equipment, the microwave frequency is 2450MHz, the power is 1000W, the control temperature is 40°C, and the microwave is irradiated for 20 minutes under the condition of vacuum degree of 0.08MPa to obtain substance A;
[0036] 2) Add 95% ethanol to substance A, the weight ratio of substance A to 95% ethanol is 1:15, under the condition that the microwave frequency is 2450MHz, the power is 1000W, the temperature is 65°C, and the stirring speed is 60 rpm under microwave-assisted reflux extraction for 40 minutes, then suction-filtered under the condition of 0.08M...
Embodiment 3
[0040] A method for microwave-assisted extraction of solanesol in potato stem and leaf waste of the present invention comprises the following steps:
[0041] 1) Get potato stems and leaves, pulverize, cross 40 mesh sieves, add 95% ethanol and stir evenly, the weight ratio of described potato stems and leaves and 95% ethanol is 1: 1, put the mixed solution of potato stems and leaves and 95% ethanol In the microwave drying equipment, the microwave frequency is 2450MHz, the power is 1500W, the control temperature is 30°C, and the microwave is irradiated for 10 minutes under the condition of vacuum degree of 0.08MPa to obtain substance A;
[0042] 2) Add 95% ethanol to substance A, the weight ratio of substance A to 95% ethanol is 1:5, under the condition that the microwave frequency is 2450MHz, the power is 1500W, the temperature is 45°C, and the stirring speed is 100 rpm under microwave-assisted reflux extraction for 30 minutes, and then suction-filtered under the condition of 0...
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