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Detection method of Naoan capsules

A detection method and capsule technology, which can be used in measuring devices, pharmaceutical formulas, and medical preparations containing active ingredients, etc., can solve the problems of large influence on the production process of curative effect, threats to drug safety and effectiveness, and incomplete qualitative and quantitative detection. And other issues

Active Publication Date: 2011-11-02
安徽雷允上药业有限公司
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AI Technical Summary

Problems solved by technology

[0009] The preparation method of Nao'an Capsules is complicated, and its curative effect is greatly affected by the quality and content of the medicinal materials and the manufacturing process of the medicine. Safety and efficacy of medicines use pose a threat

Method used

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Embodiment Construction

[0039] The present invention will be further described in detail through specific examples below.

[0040] The detection method of the present invention mainly includes four links of observation, identification, inspection and content determination. The observation is the observation of powder properties, that is, taking Naoan Capsules for observation. The content should be brown to tan granular powder; the smell is fragrant and the taste is bitter.

[0041] 【identification】

[0042] (1) Identification of Rhizoma Chuanxiong and Angelica in the prescription by TLC

[0043] Take 5g of the content of this product, add 40ml of ether, extract under reflux for 1 hour, discard the ether solution, evaporate the dregs to dry the solvent, add about 1ml of concentrated ammonia test solution to make it wet, add 40ml of chloroform, extract under reflux for 2 hours, filter, The filtrate was evaporated to dryness, and the residue was dissolved in 1ml of ethanol as the test solution. In ad...

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Abstract

The present invention provides a detection method of Naoan capsules, comprising the following steps of: (A) observing characteristics of powder; (B) identifying medicinal materials of Szechuan lovage rhizome and angelica in a prescription by a thin-layer chromatography method; (C) identifying ginseng in the prescription by the thin-layer chromatography method; (D) ensuring that inspection should accord with the provisions of the capsules, according to the appendix IL of Chinese Pharmacopoeia (2005 version); (E) measuring the ferulic acid content in the prescription by adopting a high performance liquid chromatography method; and (F) measuring the ginsenoside content in the prescription by adopting the high performance liquid chromatography method. By adopting the method, the invention can well detect the ingredients and the content of the Naoan capsules qualitatively and quantitatively and ensure the medicine quality, thereby improving the security and the effectiveness of the medicine use.

Description

technical field [0001] The invention relates to the technical field of drug inspection, in particular to a method for detecting Nao'an capsules. Background technique [0002] Traditional Chinese patent medicine detection methods can only qualitatively describe the composition of Chinese patent medicines. Efficient and quantitative detection of Chinese patent medicine components is a technical problem that the modern Chinese medicine industry needs to solve urgently. [0003] Nao'an Capsules are made of five natural medicines through a series of processes such as crushing, purification, filtration, decoction, and drying. , It has a good curative effect on hemiplegia, crooked tongue, partial body numbness, drooling at the corners of the mouth, insufficient blood supply to the brain, and can also prevent stroke. [0004] Nao'an Capsules are hard capsules, and the contents are brown to tan granular powder; the gas is fragrant and the taste is bitter. It is mainly made of Chuan...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N30/02G01N30/36A61K36/286A61P9/10A61K31/045
Inventor 赵玉龙
Owner 安徽雷允上药业有限公司
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