Extraction method of ophiopogon root, ginseng and shiandra and preparation thereof
The technology of Schisandra chinensis and ginseng is applied in the field of preparations for invigorating Qi and Fumai for the treatment of cardiovascular diseases and the field of preparation thereof, and achieves the effects of low cost, low dosage and easy storage for a long time.
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Embodiment 1
[0061] Combined extraction of ginseng and schisandra, the extraction steps are as follows:
[0062] Add water to the medicinal material, adjust the pH to 9, decoct three times, 30 minutes each time, combine the extracts and concentrate; refrigerate and precipitate with 75% ethanol and 85% ethanol successively, filter, recover ethanol under reduced pressure until the relative density is 1.1-1.20, The obtained product is a compound extract.
[0063] Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0064] Mix the raw materials of traditional Chinese medicine with water and heat them with microwave at 70W for 20 minutes. The liquid-solid mass ratio of water and Ophiopogon japonicus is 60:1. The obtained product is a single extract, and the above combined extract and single extract are combined Get the extract.
Embodiment 2
[0066] Combined extraction of ginseng and schisandra, the extraction steps are as follows:
[0067] Add water to the medicinal material, adjust the pH to 14, decoct three times, 1 hour each time, combine the extracts and concentrate; refrigerate and precipitate with 75% ethanol and 85% ethanol successively, filter, recover ethanol under reduced pressure until the relative density is 1.1-1.20, The obtained product is a compound extract.
[0068] Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0069] Mix the raw materials of traditional Chinese medicine with water and heat them with microwave at 70W for 20 minutes. The liquid-solid mass ratio of water and Ophiopogon japonicus is 60:1. The obtained product is a single extract, and the above combined extract and single extract are combined Get the extract.
[0070] The above combined extracts and single extracts were combined to obtain extracts.
Embodiment 3
[0072] Combined extraction of ginseng and schisandra, the extraction steps are as follows:
[0073] Add water to the medicinal material, adjust the pH to 12, decoct three times, 1 hour each time, combine the extracts and concentrate; refrigerate and precipitate with 75% ethanol and 85% ethanol successively, filter, recover ethanol under reduced pressure until the relative density is 1.1-1.20, The product obtained is a composite extract,
[0074] Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0075] Take Ophiopogon japonicus medicinal material and percolate with 90% ethanol, remove alcohol after percolation, extract with water 3 times in the usual way, each time for 40 minutes, filter while hot, add 0.2% activated carbon to the filtrate, stir evenly, let stand overnight; filtrate decarbonized extraction Concentrate the solution under reduced pressure to 1 / 10 of the original volume, add 95% ethanol for ethanol analysis, so that the alco...
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