Method for extracting radix ophiopogonis, ginseng and schisandra chinensis as well as preparation thereof
A technology of schisandra chinensis and ginseng, applied in the field of Yiqi Fumai preparation for treating cardiovascular diseases and its preparation, can solve the problems of low extraction rate, high cost, complicated production process, etc., and achieve high extraction rate, low cost, and high curative effect Effect
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Embodiment 1
[0058] Combined extraction of ginseng and schisandra, the extraction steps are as follows:
[0059] Add water to the medicinal material, adjust the pH to 9, decoct three times, 30 minutes each time, combine the extracts and concentrate; successively use 75% ethanol and 85% ethanol to refrigerate and precipitate, filter, and recover ethanol under reduced pressure until the relative density is 1.1-1.20 , the product obtained is a composite extract.
[0060] Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0061] Take the medicinal material and extract it once with 80% ethanol for 30 minutes each time. After filtering, add water to the filter residue and decoct for extraction twice, each time for 1 hour. The extract is ultrafiltered with an ultrafiltration membrane with a cut-off molecular weight of 30,000, and the effluent is collected. , concentrated under reduced pressure, the product obtained is a single extract, and the above combined...
Embodiment 2
[0063] Combined extraction of ginseng and schisandra, the extraction steps are as follows:
[0064] Add water to the medicinal material, adjust the pH to 14, decoct three times, 1 hour each time, combine the extracts and concentrate; successively refrigerate and precipitate with 75% ethanol and 85% ethanol, filter, and recover ethanol under reduced pressure until the relative density is 1.1-1.20 , the product obtained is a composite extract.
[0065] Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0066] Take the medicinal material and extract it with 95% ethanol for 3 times, each time for 1 hour. After filtering, add water to the filter residue and decoct for 3 times, each time for 2 hours. The extract is ultrafiltered with an ultrafiltration membrane with a molecular weight cut-off of 100,000, and the effluent is collected. , concentrated under reduced pressure, the product obtained is a single extract,
[0067] The combination of t...
Embodiment 3
[0069] Combined extraction of ginseng and schisandra, the extraction steps are as follows:
[0070] Add water to the medicinal material, adjust the pH to 12, decoct three times, 1 hour each time, combine the extracts and concentrate; successively use 75% ethanol and 85% ethanol to refrigerate and precipitate, filter, and recover ethanol under reduced pressure until the relative density is 1.1-1.20 , the product obtained is a composite extract.
[0071] Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0072] Take the medicinal material and extract it twice with 90% ethanol for 1 hour each time. After filtering, add water to the filter residue and decoct it for 3 times, 2 hours each time. The extract is ultrafiltered with an ultrafiltration membrane with a cut-off molecular weight of 60,000, and the effluent is collected. , concentrated under reduced pressure, the product obtained is a single extract,
[0073] The combination of the abov...
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