Colored and transparent heat-insulating energy-saving protecting function coating and preparation method thereof
A protective function and color technology, applied in the direction of coating, etc., can solve the problems of light absorption and heat generation
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Embodiment 1
[0122] The preparation of embodiment 1nm_Ce-ATO / nm_Y-ITO composite dispersion liquid
[0123] Step 1: Preparation of experimental equipment and materials
[0124] 1. Experimental equipment: 2000mL glass beaker; electronic scale; LBM-T1 type adjustable speed and frequency conversion mixing and dispersing machine (manufactured by Hong Kong Langling Machinery Co., Ltd.); ).
[0125] 2. Experimental materials: nano antimony tin oxide (the following abbreviation is nm_ATO); rare earth nano-cerium oxide (the following abbreviation is nm_CeO); polyvinyl alcohol (PVA) / (chemical pure reagent); NK-1 (neutral) super Dispersant (Zhejiang Deqing Baowei Nano Material Co., Ltd.); BYK-2100 (water-based) and BYK-136 (oily) anionic dispersant; propylene glycol methyl ether acetate (PMA) / (chemical pure reagent); AC1261 acrylic resin ( Produced by Foshan Gaoming Tongde Chemical Co., Ltd.).
[0126] Step 2: Preparation of aqueous nanodispersion
[0127] First use a graduated 2000mL glass beake...
Embodiment 2
[0130] The preparation of embodiment 2nm_Y-ITO composite color paste
[0131] Preparation of experimental equipment and materials for the first step
[0132] 1. Experimental equipment is the same as embodiment 1.
[0133] 2. Experimental materials nano-oxide (nm_ITO); nano-rare earth oxide YO (nm_YO); phthalocyanine blue (commercially available); phthalocyanine green (commercially available) R-960 titanium dioxide (DuPont); pigment scarlet (commercially available); Iron oxide red (commercially available); iron oxide black (commercially available); fast yellow (commercially available); polyvinyl alcohol (PVA) / (commercially available) NK-1 hyperdispersant (Zhejiang Deqing Baowei Nano Material Co., Ltd. ); JF-134 cationic fluorosurfactant and F-006 amphoteric fluorosurfactant (produced by Wuhan Jinfu Technology Development Co., Ltd.); NDZ-311W (water-based) / NDZ-311 (oil-based) titanate coupling agent (Nanjing Shuguang Chemical Group); propylene glycol methyl ether acetate (PMA)...
Embodiment 3
[0139] Synthesis of embodiment 3nm_Ce-ATO modified silicone acrylic resin
[0140] The configuration of experimental equipment and materials for the first step:
[0141] 1) The experimental equipment is equipped with a four-necked flask reactor with a reflux condenser, an electric stirrer, a constant pressure dropping funnel and a thermometer; a storage tank (steel cylinder) filled with nitrogen; an electric heating furnace with an asbestos protective cover and other experiments Measuring instruments and appliances used in the room, etc.
[0142] 2) Experimental materials Ethyl acrylate (EA), butyl acrylate (BA), methyl methacrylate (MMA), hydroxypropyl acrylate (HPA), dodecyl mercaptan (NDM), propylene glycol methyl ether acetate (PMA), butyl acetate (BAC), n-butanol (BTL), initiator (BPO, benzoyl peroxide), ethyl silicate-40, ethanol, catalyst SF-10 (by mass ratio: n-butyl Alcohol:hydrochloric acid=95:5 mixed, both are chemically pure reagents). Except for SF-10 which is ...
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