Technology for granulating powder
A powder and system technology, applied in the direction of granulation of special binders, etc., can solve the problems of high mechanical performance requirements, poor surface finish, and low sphericity of particles, and achieve low equipment requirements, smooth surface, and high ball formation rate. Effect
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Embodiment 1
[0023] Weigh 3g of hydroxyethyl cellulose, heat to dissolve in 240mL deionized water, add 80g of acrylamide and 16g of N,N-methylenebisacrylamide to dissolve completely, then add 100g of zirconium dioxide powder to make the powder The solid was dispersed evenly in the solution, and finally 0.4 g of ammonium persulfate was added and stirred evenly. Add 1200mL of chlorobenzene and 36g of Span-40 into a clean 3000mL three-necked glass reactor, and stir to dissolve the Span-40 completely. Slowly pour the above-mentioned water phase containing zirconia powder into the three-port reaction kettle, adjust the stirring speed so that the particle size of the balls is between 0.3mm-1mm, then control the speed unchanged, slowly raise the temperature to 60°C and keep it for 3 hours to make the balls The beads were solidified, and then the temperature was raised to 90°C for 3 hours to complete the reaction. After extraction and sieving, 250 g of spherical particles with a qualified particl...
Embodiment 2
[0025] Weigh 2.4g of carboxymethylcellulose, heat to dissolve in 240mL of deionized water, add 200g of acrylamide and 40g of N,N-methylenebisacrylamide to dissolve completely, then add 360g of zirconium dioxide powder to make The powder is evenly dispersed in the solution, and finally 4.8 g of ammonium persulfate is added and stirred evenly. Add 1200mL chlorobenzene and 120g Span-40 into a clean 3000mL three-necked glass reactor, stir to dissolve the Span-40 completely. Slowly pour the above-mentioned water phase containing zirconia powder into the three-port reaction kettle, adjust the stirring speed so that the particle size of the balls is between 0.3mm-1mm, then control the speed unchanged, slowly raise the temperature to 60°C and keep it for 3 hours to make the balls The beads were solidified, and then the temperature was raised to 80° C. for 5 hours to complete the reaction. After extraction and sieving, 600 g of spherical particles with a qualified particle size were o...
Embodiment 3
[0027] Weigh 0.6g of hydroxyethyl cellulose, heat to dissolve in 120mL of deionized water, add 10g of acrylamide and 2g of N,N-methylenebisacrylamide to dissolve completely, then add 6g of zirconium dioxide powder to make The powder is evenly dispersed in the solution, and finally 0.3 g of ammonium persulfate is added and stirred evenly. Add 1200mL of chlorobenzene and 36g of Span-40 into a clean 3000mL three-necked glass reactor, and stir to dissolve the Span-40 completely. Slowly pour the above-mentioned water phase containing zirconia powder into the three-port reaction kettle, adjust the stirring speed so that the particle size of the balls is between 0.3mm-1mm, then control the speed unchanged, slowly raise the temperature to 60°C and keep it for 3 hours to make the balls The beads were solidified, and then the temperature was raised to 90°C for 3 hours to complete the reaction. After extraction and sieving, 25 g of spherical particles with a qualified particle size were...
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