PtNi alloy/graphene combined nanometer catalyst with hollow structure and preparation method thereof
A graphene composite and nano-catalyst technology, applied in metal/metal oxide/metal hydroxide catalysts, physical/chemical process catalysts, chemical instruments and methods, etc. Catalyst interaction and other issues, to achieve excellent electron conductivity, excellent catalytic performance, the effect of reducing dosage
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Embodiment 1
[0034] 1 mg graphene oxide was ultrasonically dispersed in 10 mL of polyvinylpyrrolidone (PVP) aqueous solution with a concentration of 10 g / L, and then 10 mL of nickel chloride solution with a concentration of 2 mmol / L was added, magnetically stirred, and high Pure nitrogen for 15 min. Then the temperature was controlled at 25 °C, and 30 mL of newly prepared sodium borohydride solution with a concentration of 50 mmol / L was added dropwise. Potassium acid solution, after the dropwise addition, continue to stir and react for 2 h. The reaction product was centrifuged, washed, and dried at 60 °C to obtain a hollow structure PtNi alloy / graphene composite nanocatalyst. The particle size of the PtNi nanoalloy hollow sphere was 10-50 nm, and the ratio of the amount of Pt to Ni was 5:1.
Embodiment 2
[0036]1 mg graphene oxide was ultrasonically dispersed in 10 mL of 20 g / L polyvinylpyrrolidone (PVP) aqueous solution, then 15 mL of 2 mmol / L nickel chloride solution was added, magnetically stirred, and high Pure nitrogen for 15 min. Then the temperature was controlled at 25 °C, and 30 mL of newly prepared sodium borohydride solution with a concentration of 50 mmol / L was added dropwise. Potassium acid solution, after the dropwise addition, continue to stir and react for 2 h. The reaction product was centrifuged, washed, and dried at 60 °C to obtain a hollow structure PtNi alloy / graphene composite nanocatalyst. The particle size of the PtNi nanoalloy hollow sphere was 10-50 nm, and the ratio of the amount of Pt to Ni was 3:1.
Embodiment 3
[0038] 2 mg graphene oxide was ultrasonically dispersed in 10 mL of 30 g / L polyvinylpyrrolidone (PVP) aqueous solution, then 20 mL of 2 mmol / L nickel chloride solution was added, magnetically stirred, and high-purity Nitrogen for 15 min. Then the temperature was controlled at 35 °C, and 20 mL of newly prepared sodium borohydride solution with a concentration of 50 mmol / L was added dropwise. Potassium acid solution, after the dropwise addition, continue to stir and react for 2 h. The reaction product was centrifuged, washed, and dried at 60 °C to obtain a hollow structure PtNi alloy / graphene composite nanocatalyst. The particle size of the PtNi nanoalloy hollow sphere was 10-50 nm, and the ratio of the amount of Pt to Ni was 2:1.
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