Leakage-proof speed reducer lubricating grease composition and preparation method thereof

A technology of reducer and lubricating grease, which is applied in the field of reducer grease, can solve the problems of unreasonable structure design of reducer, ineffective effect, hidden dangers of equipment accidents, etc., achieve good colloidal stability and thixotropy, and simple process and equipment , the effect of reducing production costs

Active Publication Date: 2012-05-02
CHINA PETROLEUM & CHEM CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Reducer oil leakage is a common problem in various enterprises, which not only increases the consumption cost of lubricating oil for enterprises, increases the labor intensity of workers, increases the probability of equipment damage, but also causes hidden dangers of major equipment accidents
The reasons for the oil leakage of the closed reducer are mainly as follows: the accumulation of heat generated by the gear meshing significantly increases the pressure in the box, forcing the lubricating oil to seep out; the sealing technology cannot meet the requirements for use; the structure design of the reducer is unreasonable, and the oil return is not smooth; The use

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0033] Example 1:

[0034] Put 15 grams of 12-hydroxystearic acid, 15 grams of stearic acid and 400 grams of paraffin-based mineral base oil into the reaction kettle, raise the temperature to 80°C, add 4.5 grams of aqueous solution of lithium hydroxide, and the amount of water added is 25 Grams. Warm up to 90℃ to start timing saponification, 1.5 hours after saponification, heat up after the saponification is over, use 300 grams of paraffin-based mineral base oil to cool in the reactor after heating to 210℃, when the cooling temperature is 145℃, continue to add 180 grams of ester Cooling the base oil (pentaerythritol ester), add 10 grams of calcium dinonyl sulfonate to 98℃, add 20 grams of solid anti-wear additive (tin metal powder) when the temperature drops to 79℃, wait until the temperature drops to 59℃ The finished product will be produced after three passes through the three-roll mill. The properties of the grease prepared by the process formula of the present invention are...

Example Embodiment

[0046] Example 2:

[0047] Combine 5 grams of 12-hydroxystearic acid and 35 grams of C 18 The fatty acid and 400 grams of paraffin mineral base oil were put into the reaction kettle, the temperature was raised to 85°C, and 6.5 grams of lithium hydroxide solution was added, and the amount of water added was 35 grams. Warm up to 95℃ to start timing saponification, 1 hour after saponification, heat up after the saponification is over, use 200 grams of naphthenic mineral base oil to cool in the reactor after heating to 210℃, when the cooling temperature is 140℃, continue to add 200 grams Ester base oil (trimethylolpropane ester) is cooled, and 5 grams of barium dinonyl sulfonate is added to the temperature to 100°C. When the temperature drops to 76°C, 25 grams of solid antiwear additive (borate) is added. After the temperature drops to 60℃, the finished product will be produced after three times of oil rolling on the three-roll mill. The properties of the grease prepared by the proc...

Example Embodiment

[0059] Example 3:

[0060] Put 30 grams of C 16 Hydroxy fatty acids and 10 g of C 20 The fatty acid and 400 grams of intermediate base mineral base oil were put into the reactor, the temperature was raised to 83°C, and 5.8 grams of lithium hydroxide solution was added, and the amount of water added was 30 grams. Warm up to 100℃ to start timing saponification, 2 hours after saponification, heat up after the saponification is over, use 200g of naphthenic mineral base oil to cool in the reactor after heating up to 210℃, when the cooling temperature is 150℃, continue to add 200g The ester base oil (dioctyl sebacate) is cooled, and 6 grams of zinc naphthenate is added to the temperature to 100°C. When the temperature drops to 76°C, 24 grams of solid antiwear additive (zinc oxide) is added. The finished product will be produced after three passes through the three-roll mill at 56°C. The properties of the grease prepared by the process formula of the present invention are listed in the...

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PUM

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Abstract

The invention relates a speed reducer lubricating grease composition and a preparation method thereof. The composition comprises 69 to 80 percent of mineral base oil, 12 to 23 percent of ester base oil, 3.2 to 6 percent of thickening agent, 0.6 to 2 percent of dinonyl sulfonate or zinc naphthenate, and 1 to 2.8 percent of solid wear-resistance additive. The preparation method comprises: adding the mineral base oil into a reaction kettle, adding fatty acid, mixing, raising temperature to 80 to 85 DEG C, adding an aqueous solution of lithium hydroxide, heating to 90 to 100 DEG C, and performingsaponification for 1 to 2 hours; raising temperature to 210 DEG C, adding the mineral base oil into the reaction kettle, and quenching, wherein the quenching temperature is kept between 140 to 190 DEG C, and the quenching oil accounts for 14 to 43 percent of the total amount of the base oil; adding the ester base oil, and cooling; when the temperature is below 100 DEG C, adding the dinonyl sulfonate or zinc naphthenate, cooling to a temperature below 80 DEG C, and adding the solid wear-resistance additive; and cooling to a temperature below 60 DEG C, rolling oil by a three-roll machine for three times and filling to obtain finished speed reducer lubricating grease composition. In the invention, the lubricating grease is prepared by one-step direct reaction, the process and equipment are simple and energy-saving, and the quality of the product produced by the process is stable.

Description

technical field [0001] The invention relates to reducer lubricating grease, more precisely to a leak-proof reducer grease composition and a preparation method thereof, which has good leak-proof performance. Background technique [0002] The reducer is generally used for transmission equipment with low speed and high torque. It can reduce the power of the electric motor, internal combustion engine or other high-speed operation through the gear with a small number of teeth on the input shaft of the reducer and the large gear on the output shaft to achieve the purpose of deceleration. The specific mechanism is to use the speed converter of the gear to reduce the number of revolutions of the motor to the desired number of revolutions and obtain a larger torque. There are many types of reducers, which can be divided into gear reducers, worm gear reducers, cycloid reducers, screw lifters, stepless speed changers, high-power gear reducers and planetary reducers according to the tra...

Claims

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Application Information

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IPC IPC(8): C10M169/00C10M177/00C10N50/10C10N40/04
Inventor 吴宝杰张广辽
Owner CHINA PETROLEUM & CHEM CORP
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