Method for adsorbing and removing microscale antibiotic in livestock and poultry waste water by modified zeolite
A technology for modifying zeolite and antibiotics, which is applied in chemical instruments and methods, multi-stage water/sewage treatment, water/sludge/sewage treatment, etc. It can solve the problem of low adsorption rate, poor adsorption removal efficiency, weak adsorption selectivity, etc. problems, to achieve the effect of improved adsorption rate and efficiency, low treatment cost, and low investment in infrastructure and equipment
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Embodiment 1
[0024] Embodiment 1: (modified zeolite adsorption removes method 1 of trace antibiotics in livestock and poultry wastewater)
[0025] The method proceeds as follows:
[0026] (1) Biological pretreatment of livestock and poultry wastewater: After the wastewater collected from livestock and poultry farms is pretreated by the UASB (upflow anaerobic sludge bed)-MBR (aerobic membrane bioreactor) secondary combination process, the effluent The COD is 82 mg / L, the concentration of tetracycline antibiotics is 0.18 mg / L, and the pH is 5.0, for standby;
[0027] (2) Zeolite modification treatment: the natural zeolite and the nitric acid solution with a concentration of 25% are mixed according to the ratio of mass volume 1g: 10ml; Vacuum filtration; rinse the treated zeolite with deionized water for 3-5 times, vacuum filter and then dry in an oven at 120°C to constant weight to obtain a nitric acid modified zeolite adsorbent for future use;
[0028] (3) Adsorption treatment of livestoc...
Embodiment 2
[0030] In this example, the biological pretreatment of step (1) livestock and poultry wastewater: the COD of the effluent after biological treatment is 70 mg / liter, the concentration of tetracycline antibiotics is 0.97 mg / liter, and the pH is 6.0, for subsequent use; step (2) zeolite Modification treatment: mix natural zeolite with hydrochloric acid solution with a concentration of 50% according to the ratio of mass volume 1g: 20ml; vacuum filter the mixture and dry it in an oven at 105°C to constant weight to obtain hydrochloric acid modified zeolite adsorption agent; step (3) adsorption treatment of livestock and poultry wastewater: the hydrochloric acid modified zeolite adsorbent and the pretreated livestock and poultry wastewater are put into the closed pool according to the ratio of mass volume 1g: 2000ml, after stirring and adsorbing for 5h under the condition of 30 ℃, tetracycline The detected concentration of antibiotics was reduced to 0.09 mg / L, and the removal rate wa...
Embodiment 3
[0032] In this example, the biological pretreatment of step (1) livestock and poultry wastewater: the COD of the effluent after biological treatment is 99 mg / liter, the concentration of tetracycline antibiotics is 0.80 mg / liter, and the pH is 7.0, and it is standby; step (2) zeolite Modification treatment: mix natural zeolite with sulfuric acid solution with a concentration of 35% according to the mass volume ratio of 1g:16ml; vacuum filter the mixture and dry it in an oven at 110°C to constant weight to obtain sulfuric acid modified zeolite adsorption agent; step (3) adsorption treatment of livestock and poultry wastewater: the sulfuric acid modified zeolite adsorbent and the pretreated livestock and poultry wastewater are put into the closed pool according to the ratio of mass volume 1g: 1300ml, after stirring and adsorbing for 3h under the condition of 25 ℃, tetracycline The detected concentration of antibiotics was reduced to 0.10 mg / L, and the removal rate was 88.8%. Under...
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