A dyeing method of blended modified fine denier dyeable polypropylene fiber
A technology of blending modification and dyeing method, which is applied in the direction of dyeing method, textile and papermaking, etc., to achieve the effect of improving dye uptake rate, uniformity and color fastness
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Embodiment 1
[0056] Example 1, Preparation of blended modified fine denier dyeable polypropylene:
[0057] The first mixed monomer in the raw material is: a mixture of 59.76g of styrene and 0.24g of triethylene glycol dimethacrylate; in the second mixed monomer, each component is: 20g of styrene, methyl methacrylate 17g, 8g butyl acrylate, 5g sodium methacrylate.
[0058] in N 2 Under protection, add 3.6g of sodium lauryl sulfate and 220g of deionized water into the four-neck flask, heat and dissolve in a water bath, add 17g of the first mixed monomer, mechanically stir for 3Omin for pre-emulsification, and raise the temperature to 75°C , add 0.35g of ammonium persulfate to initiate the reaction, keep stirring until the product appears blue;
[0059] Add the remaining 43g of the first mixed monomer dropwise, control the dropping speed, finish dropping in 1.5h, and keep warm for 30min; add 0.4g ammonium persulfate, then add dropwise 50g of the second mixed monomer, control the dropping ...
Embodiment 2
[0063] Example 2, The fiber of embodiment 1, this fiber sample is dyed light red with following method, and step is as follows:
[0064] When dyeing, the blended modified fine-denier dyeable polypropylene fiber is added with water at a weight ratio of 1:40, and the dissolved cationic dye red X-GRL is added: 0.05%, and the amount of leveling agent 1227 is : 2.0%, Yuanmingfen 6.0%, the amount of acetic acid added is 0.5%. Start temperature control at 25°C. After running for 20 minutes, raise the temperature to 70°C at 0.5°C / min, and then run for 30 minutes. Subsequently, the temperature was raised to 100°C at 1.5°C / min. After running for 30 minutes, lower the temperature to 40°C at 3°C / min, drain the residual liquid, wash twice with water at 20°C, and finally dry the dyed fibers or dry them after functional finishing.
[0065] The addition amount of leveling agent, sodium sulfate and acetic acid is based on the weight of the blended modified fine-denier polypropylene fiber. ...
Embodiment 3
[0067] Example 3, Using the same method as in Example 1, 5 g of sodium methacrylate was selected as the ionic monomer to prepare a blended modified fine denier dyeable polypropylene fiber. The weight ratio of polymer core-shell structure ionic nanoparticle powder to polypropylene is 8:92, and the single filament fineness is 2dtex. The fiber sample is dyed blue by the following method:
[0068] When dyeing, add water to the blended modified fine-denier dyeable polypropylene fiber at a bath ratio of 1:35, add dissolved cationic blue SD-GSL1.0% and dispersed cationic yellow SD-5GL0.3%, Yuan Ming Powder 8%, acetic acid addition is 1.0%. Start to control the temperature at room temperature. After running for 20 minutes, raise the temperature to 70°C at 1°C / min and run for 30 minutes. Then the temperature was raised to 100°C at 1°C / min. After running for 50 minutes, lower it to 40°C at 3°C / min, drain the residual liquid, wash it twice with 40°C water, and finally dry the dyed fi...
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