Alginic acid-containing aqueous composition, alginate impression material for dental applications, and substrate for alginate impression material for dental applications
By adding non-reducing sugars, especially trehalose, to the alginic acid aqueous composition, the aggregation of alginic acid is inhibited, the problem of viscosity reduction is solved, and the stability and impression of dental alginate impression materials are improved. The mold accuracy meets the needs of long-term use.
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[0127] Hereinafter, although an Example and a comparative example are given and demonstrated in order to demonstrate this invention concretely, this invention is not limited by these Examples and a comparative example at all.
[0128] I. Evaluation of viscosity retention and hardening
Embodiment A1
[0131] 1.0 g of alginic acid (manufactured by Kimi Kei Co., Ltd., M / G ratio = 1.2) was stirred and dissolved in 1000 g of distilled water. After the alginic acid was dissolved, 10 g of trehalose was added and dissolved as a non-reducing sugar.
[0132] For the composition prepared by the above method, the viscosity in a 23° C. constant-temperature water tank was measured using a Cannon-Fenske viscometer (manufactured by Shibata Scientific Co., Ltd.), which is a kind of capillary viscometer, and was used as the viscosity immediately after production. . Then, 50 mL of the composition was filled into transparent glass bottles, the glass bottles were tightly capped, and stored in a constant temperature tank at 50° C. for seven days. The viscosity was measured again after storage for seven days, and the viscosity retention (%) was calculated from the viscosity measurement values of the composition before and after heat treatment according to the following formula (2). Table 1 sh...
Embodiment A2~A4
[0135] (Examples A2 to A4, Comparative Examples A1 to A3)
[0136] According to the method of Example A1, alginic acid-containing aqueous compositions having different compositions shown in Table 1 were prepared. Table 1 shows the results of the composition and viscosity retention of each composition. Both sodium alginate and potassium alginate used were manufactured by Himek Corporation, and both had an M / G ratio of 1.2.
[0137] [Table 1]
[0138]
[0139] In Comparative Examples A1 to A3, no non-reducing sugar was contained at all, and in any of the cases, a decrease in viscosity over time was observed. In contrast, Examples A1 to A4 contained alginic acid or its derivatives, water, and non-reducing sugars, and in any case, in comparison with Comparative Examples A1 to A3 that did not contain non-reducing sugars, all It was confirmed that the decrease in viscosity over time was suppressed.
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