Durable organic matter large-volume water sample separation and concentration device

A technology for separation and enrichment of organic matter, applied in the direction of filtration separation, separation method, preparation of test samples, etc., can solve the problems that the filter does not have an enrichment device, easy to block the filter membrane and filter plate, and waste samples, etc., to achieve Facilitate the pollution level and distribution law, improve the effect of filtration speed and efficiency

Inactive Publication Date: 2013-01-09
济南市环境保护科学研究院
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] When the laboratory enriches persistent organic compounds in liquid samples, it often uses micro-analysis filtration devices, which include liquid storage bottles, filters and receiving bottles , when there are many suspended particles in the liquid sample, it is easy to cause the filter membrane to be blocked, so the filter needs to be replaced frequently, and the experimenter has to pour out the sample in the liquid storage bottle, which greatly wastes the sample; in addition, the above filter It includes a glass funnel and a filter plate matched with the

Method used

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  • Durable organic matter large-volume water sample separation and concentration device
  • Durable organic matter large-volume water sample separation and concentration device
  • Durable organic matter large-volume water sample separation and concentration device

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Embodiment Construction

[0016] A large-volume water sample separation and enrichment device for persistent organic matter, including a liquid storage bottle 3 and a filter 6 that is movably connected to the liquid storage bottle 3 through a clip 5, and a top cover 2 with a water inlet is provided above the liquid storage bottle 3 , the water inlet is connected to the sampling tube 1; the above device also includes a receiving bottle 8 connected to the filter 6 through a rubber stopper 7, and the rubber stopper 7 seals the receiving bottle 8, between the receiving bottle 7 and the vacuum pump 11 A safety bottle 10 with anti-suckback is connected, and the sample inlet tube in the safety bottle 10 is lower than the position of the sample outlet tube; there is a locking piston 4 with a hole at the lower bottle mouth of the liquid storage bottle 3, and the locking piston 4 can be used at any time. Control whether the sample solution is injected into the filter 6; there is a scale 9 on the receiving bottle ...

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Abstract

The invention belongs to the field of an environmental water sample separation and concentration device, and particularly relates to a durable organic matter large-volume water sample separation and concentration device. The device comprises a liquid storage bottle, and a filter, a receiving bottle, a safety bottle and a vacuum pump, which are movably connected with the liquid storage bottle, wherein a top cover with a water inlet is arranged above the liquid storage bottle, and the water inlet is connected with a sample feeding pipe; a safety bottle is arranged between the receiving bottle and the vacuum pump; and the filter is provided with two layers of filter plates, a sand core is clamped inside an intubation tube below a glass funnel, and a concentration layer is arranged above the sand core. Due to the adoption of the device, the samples can be separated and concentrated on the sampling field; and since the filter is provided with the two layers of filter plates, and the concentration layer is arranged inside the intubation tube, not only can suspended particles containing the durable organic matters be separated and the filter speed and filter efficiency be improved, but also the dissolved durable organic matters can be effectively concentrated, so that the pollution level and the distribution principle of the durable organic matters in two phases of the environmental water sample can be more conveniently researched.

Description

technical field [0001] The invention belongs to the field of environmental water sample separation and enrichment devices, and in particular relates to a persistent organic matter large-volume water sample separation and enrichment device. Background technique [0002] When the laboratory enriches the persistent organic matter in the liquid sample, the micro-analysis filtration device is often used. The device includes a liquid storage bottle, a filter and a receiving bottle. When there are many suspended particles in the liquid sample, it is easy to cause the filter membrane to be blocked. , so the filter needs to frequently replace the filter membrane, and the experimenter has to pour out the sample in the liquid storage bottle, which greatly wastes the sample; in addition, the above-mentioned filter includes a glass funnel and a filter plate matched with the funnel. , Lay a glass fiber filter membrane on the filter plate, the liquid sample is filtered through the filter m...

Claims

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Application Information

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IPC IPC(8): G01N1/40B01D36/02B01D36/00
Inventor 李海滨张厚勇杜世勇王在峰
Owner 济南市环境保护科学研究院
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