Preparation method of CuSn10Bi3.5 copper-bismuth alloy powder
A powder preparation and alloy powder technology, which is applied in the field of CuSn10Bi3.5 copper-bismuth alloy powder preparation, can solve environmental pollution and other problems
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[0018] refer to figure 1 , shows the flow chart of the steps of the CuSn10Bi3.5 copper-bismuth alloy powder preparation method of the embodiment of the present invention, which includes the following steps:
[0019] S1, select copper Cu with a weight percentage of 85-88%, 9-11% tin Sn, and 3-4% bismuth Bi as raw materials, add Cu to a smelting furnace and heat to 1080°C in the atmosphere for melting, and wait After the copper is melted, Sn is added, and Bi is smelted to form an alloy liquid. The smelting temperature is 1100-1120°C, and the smelting time is 15-20 minutes;
[0020] S2. After removing slag on the liquid surface, the composition detection of the alloy liquid is controlled at Cu85-88%, Sn9-11%, Bi3-4%, and the inevitable or unremovable impurities are ≤0.3%. After the composition test is qualified, the temperature is raised to 1150-1180 ℃;
[0021] S3, remove the slag, inject the alloy liquid into the leakage bag, use the free-falling rectangular ring hole nozzle ...
Embodiment 1
[0027] A method for preparing CuSn10Bi3.5 copper-bismuth alloy powder, comprising the following steps:
[0028] (1) Select the raw material weight percentage components as follows: 1# electrolytic copper 86.5%, 1# tin ingot 10%, 99.95# bismuth ingot 3.5%, specifically adopt 0.25T intermediate frequency smelting furnace, take 1# electrolytic copper 216.25Kg, 1# tin ingot 25Kg, 99.95# bismuth ingot 8.75Kg, first add Cu and heat to 1080°C in the atmosphere for melting, then add Sn and Bi for melting to obtain alloy liquid after Cu is melted, the melting temperature is 1100-1120°C, The melting time is 15-20 minutes.
[0029] (2) After the slag removal on the liquid surface of the alloy liquid, the composition detection is controlled at Cu85-88%, Sn9-11%, Bi3-4%, and the inevitable or unremovable impurities are ≤0.3%, and the temperature is raised to 1150-1180 after passing the composition detection ℃.
[0030] (3) Remove the slag, inject the alloy liquid into the leakage bag, an...
Embodiment 2
[0035] A preparation method of CuSn10Bi3.5 copper-bismuth alloy powder, which comprises the following steps:
[0036] (1) The weight percentage of raw materials is selected as follows: 1# electrolytic copper 85%, 1# tin ingot 11%, 99.95# bismuth ingot 4%, the raw material Cu is added to the smelting furnace and heated to 1080 ° C in the atmosphere for melting. After Cu is melted, Sn and Bi are added for smelting, the smelting temperature is 1100-1120°C, and the smelting time is 15-20 minutes.
[0037] (2) After removing slag from the alloy liquid surface, the composition detection is controlled at Cu85-88%, Sn9-11%, Bi3-4%, and the unavoidable or unremovable impurities are ≤0.3%. .
[0038] (3) Remove the slag, inject the alloy liquid into the leakage bag, and use the free-falling rectangular ring hole nozzle to atomize with 4MPa water pressure under the protection of inert gas. The high-pressure water temperature is controlled at 48°C, and the high-pressure water flow crushe...
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