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Method for preparing hydrophobic lipophilic cotton fabric material through structuring zinc oxide fine structure

A microstructure, hydrophobic and lipophilic technology, applied in chemical instruments and methods, physical treatment, plant fibers, etc., can solve the problems that are rarely reported, and achieve good oil absorption capacity and good application value

Active Publication Date: 2013-10-09
SHANGHAI UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, Zhang Qi et al. explored the preparation of zinc oxide nanostructures, showed good nanostructures, and tested its electrical conductivity and other properties, but there are still few studies on the preparation of superhydrophobic cotton fabric surfaces using the fine structure of zinc oxide nanocrystals. to report

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0012] 1. Material preparation

[0013] (1) Preparation of reagents

[0014] The main reagents are: palmitic acid (hexadecanoic acid), absolute ethanol (CH 3 CH 2 OH), sodium hydroxide (NaOH), glacial acetic acid (CH 3 COOH), hexamethylenetetramine (C 6 h 12 N 4 ), zinc nitrate (Zn(NO 3 ) 2 ·6H 2 O), zinc acetate (Zn(CH 3 COO) 2 2H 2 O).

[0015] (2) Tested cotton fabric

[0016] Cotton plain weave, purchased locally.

[0017] (3) Experimental instruments and equipment

[0018] Constant temperature magnetic stirrer, oven, ultrasonic cleaning machine.

[0019] 2. The specific process of preparing materials is:

[0020] a. Prepare 0.05mol / L zinc acetate alcohol solution at 60~65℃, add 0.10~0.15mol / L sodium hydroxide alcohol solution drop by drop under stirring until a transparent zinc oxide colloid with Tyndall phenomenon is formed solution;

[0021] b. Soak the cleaned cotton fabric in the colloidal solution of zinc oxide obtained in step a for 2-5 minutes, th...

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Abstract

The invention relates to a method for preparing a hydrophobic lipophilic cotton fabric material through structuring a zinc oxide fine structure. The method comprises the following steps of: combining a sol-gel method with a hydrothermal method, i.e. uniformly laying prepared zinc oxide nano seed crystals on the surface of a cotton fabric through utilizing the sol-gel method at first, then growing zinc oxide nanorods toward fixed directions on the surface of the cotton fabric through utilizing the hydrothermal method, finally, modifying the cotton fabric through utilizing long-chain fatty acid-palmitic acid so as to have superhydrophobicity, and wrapping cotton with the cotton fabric for oil absorption. According to the method, the specific structure of zinc oxide is utilized to structure the superhydrophobic cotton fabric surface, and moreover, the cotton fabric has lipophilicity, good oil absorption after wrapping the cotton and a good practical application value in petroleum pollution water body remediation.

Description

technical field [0001] The invention relates to a method for preparing a hydrophobic and lipophilic cotton fabric material, in particular to a method for preparing a hydrophobic and lipophilic cotton fabric material by constructing a zinc oxide microstructure. Background technique [0002] In nature, superhydrophobic phenomena are ubiquitous, and the most typical example is the surface of various plant leaves represented by lotus leaves. Hydrophobic surfaces have attracted widespread interest. In addition to the leaves of plants, the bodies of many animals have superhydrophobic properties, such as the wings of butterflies and the feathers of waterfowl. The urgent need for functional materials has drawn great attention to the application of microstructures in life science and material science, and the relationship between microstructures and wettability of solid surfaces has aroused widespread interest among scientists. Superhydrophobicity is an extreme special case of surf...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/44D06M13/188D06M10/04C09K3/32D06M101/06
Inventor 李辈辈刘晓艳张新颖邹君臣柴文波王倩李红兵
Owner SHANGHAI UNIV
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