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Advanced chemical synthesis of dibenzyltoluene heat transfer liquid and preparation method thereof

A dibenzyltoluene, chemical synthesis technology, applied in the field of advanced chemical synthesis of dibenzyltoluene heat transfer fluid and its preparation, can solve the problems of poor high temperature resistance, reduced service life, poor thermal conductivity, etc., and achieve long life , Excellent high temperature resistance, good heat transfer performance

Active Publication Date: 2016-03-30
SHANDONG ENKLI CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, in the normal production process in the chemical industry, it is often necessary to heat the reactor, etc., so the use of heat transfer oil has become inevitable in the chemical industry. Of course, not only in the chemical industry, the use of heat transfer oil is becoming wider and wider. It It has excellent heat conduction performance, and at the same time, through the conduction of heat transfer oil, the objects that need to receive heat are heated evenly, ensuring the normal progress of the reaction, etc. However, the high temperature resistance of the current conduction fluids on the market is not good. When the temperature is high, the performance of the heat transfer oil will change. When the temperature is too high, the performance of the heat transfer oil will be unstable, the service life will be reduced, and the heat conduction effect will be poor.

Method used

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  • Advanced chemical synthesis of dibenzyltoluene heat transfer liquid and preparation method thereof
  • Advanced chemical synthesis of dibenzyltoluene heat transfer liquid and preparation method thereof
  • Advanced chemical synthesis of dibenzyltoluene heat transfer liquid and preparation method thereof

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Embodiment 1

[0014] Advanced chemical synthesis of dibenzyltoluene heat transfer fluid is prepared by adding functional additives to dibenzyltoluene, wherein the functional additives are made of the following raw materials in mass percentages:

[0015]

[0016] The addition amount of the functional aid is 1.5% of the mass of the mixture of alkylbenzenes.

[0017] KX-ZJ-01 high temperature coking inhibitor is produced by Shandong Kexin Petrochemical Co., Ltd.

[0018] KX-ZS-03 hydrogenation scale inhibitor is produced by Shandong Kexin Petrochemical Co., Ltd.

[0019] The preparation method of the advanced chemical synthesis dibenzyltoluene heat transfer fluid is: adding functional additives into the dibenzyltoluene mixture according to the proportion, and fully merging by ultrasonic wave or mechanical stirring to obtain the finished product.

[0020] The product performance is shown in the table below.

[0021]

[0022]

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PUM

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Abstract

The invention relates to advanced chemically synthesized dibenzyltoluene heat transfer fluid and a preparation method thereof. The method belongs to the field of chemical engineering heat transfer oil. The method is characterized in that the fluid is prepared by adding a functional auxiliary agent into dibenzyltoluene. The functional auxiliary agent is prepared from the raw materials of, by mass: 30% of a high-temperature antioxidant alkyldiphenylamine, 30% of a detergent sulfurized alkylphenol calcium, 30% of base synthetic calcium sulfonate in the detergent, 4% of a KX-ZJ-01 high-temperature scorch resisting agent, and 6% of a KX-ZS-03 hydrogenation inhibitor. The heat transfer fluid has excellent high-temperature resistance, and can resist temperature up to 400 DEG C. The material is a currently best heat carrier which is better than that of a national standard. The material is safe and environment-friendly, and has the advantages of good heat transferring performance and long service life.

Description

technical field [0001] The invention relates to an advanced chemically synthesized dibenzyltoluene heat transfer fluid and a preparation method thereof, belonging to the field of chemical heat transfer oil preparation. Background technique [0002] At present, in the normal production process in the chemical industry, it is often necessary to heat the reactor, etc., so the use of heat transfer oil has become inevitable in the chemical industry. Of course, not only in the chemical industry, the use of heat transfer oil is becoming wider and wider. It It has excellent heat conduction performance, and at the same time, through the conduction of heat transfer oil, the objects that need to receive heat are heated evenly, ensuring the normal progress of the reaction, etc. However, the high temperature resistance of the current conduction fluids on the market is not good. When the temperature is high, the performance of the heat transfer oil will change. When the temperature is too...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K5/10
Inventor 刘富春
Owner SHANDONG ENKLI CHEM