A kind of fracture-resistant composite glass material and its preparation method
The invention relates to a composite glass and anti-fracture technology, which is applied in the field of glass materials with good anti-fracture properties and its preparation, which can solve problems such as broken and achieve the effect of improving anti-fracture properties.
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Embodiment 1
[0012] A method for preparing a fracture-resistant composite glass material, the preparation method comprising the following steps: (1) The raw material components for preparing glass are respectively: P 2 o 5 5kg, BaO 6kg, Sb 2 o 3 5kg, Na 2 O is 8kg, MgO is 13kg, SiO 2 Take the corresponding raw materials of each of the above ingredients and mix them at room temperature; (2) Grind each of the above corresponding raw materials through a pulverizer, pass through a 300-mesh sieve after crushing, and ventilate and dry after sieving. The drying time is 0.5h ; (3) After drying, put the 300-mesh mixed ingredient raw material into a quartz crucible and heat it to 1180°C. During the heating process, the heating rate of the crucible is 70°C / min. After the temperature is constant, keep it warm for 5 hours, and stir while keeping it warm; (4) After stirring, ventilate for clarification; (5) pour the composite glass material into the mold after clarification; (6) anneal after pouring...
Embodiment 2
[0014] A method for preparing a fracture-resistant composite glass material, the preparation method comprising the following steps: (1) The raw material components for preparing glass are respectively: P 2 o 5 7kg, BaO 4kg, Sb 2 o 3 6kg, Na 2 O is 12kg, MgO is 10kg, SiO 2 Take the corresponding raw materials of each of the above ingredients and mix them at room temperature; (2) Grind the above corresponding raw materials through a pulverizer, pass through a 300-mesh sieve after crushing, and ventilate and dry after sieving. The drying time is 0.5h ; (3) After drying, put the 300-mesh mixed ingredient raw material into a quartz crucible and heat it to 1220°C. During the heating process, the heating rate of the crucible is 70°C / min. After the temperature is constant, keep it warm for 5 hours, and stir while keeping it warm; (4) After stirring, ventilate for clarification; (5) pour the composite glass material into the mold after clarification; (6) anneal after pouring, keep ...
Embodiment 3
[0016] A method for preparing a fracture-resistant composite glass material, the preparation method comprising the following steps: (1) The raw material components for preparing glass are respectively: P 2 o 5 10kg, BaO 3kg, Sb 2 o 3 4kg, Na 2 O is 10kg, MgO is 11kg, SiO 2 Take the corresponding raw materials of each of the above ingredients and mix them at room temperature; (2) Grind the above-mentioned corresponding raw materials through a pulverizer, pass through a 300-mesh sieve after crushing, and ventilate and dry after sieving. The drying time is 0.5h (3) After drying, put 300-mesh mixed ingredients into a quartz crucible and heat to 1260°C. During the heating process, the heating rate of the crucible is 70°C / min. After the temperature is constant, keep it for 5 hours, and stir while keeping it; (4) After stirring, ventilate for clarification; (5) pour the composite glass material into the mold after clarification; (6) anneal after pouring, keep it at 900°C for 2 ho...
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