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A kind of secondary utilization method of nickel plating waste liquid

A waste liquid and nickel plating technology, which is applied in liquid chemical plating, metal material coating process, coating, etc., can solve the problems of increasing sewage treatment cost, waste of resources, costing a lot of manpower and material resources, etc., to reduce the cost of sewage treatment , to avoid the effect of wasting resources

Active Publication Date: 2017-02-22
CHINA ZHENHUA GRP YONGGUANG ELECTRONICS CO LTD STATE OWNED NO 873 FACTORY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, no matter whether acidic nickel plating or alkaline plating solution is used, the plating solution is only used once, and the remaining waste plating solution is poured out. The plating solution contains harmful substances, which cannot be directly discharged into rivers according to environmental protection requirements. It takes a lot of manpower and material resources to process and meet environmental protection requirements before it can be discharged. This not only causes waste of resources, but also increases the cost of sewage treatment.

Method used

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Examples

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Effect test

Embodiment Construction

[0016] A secondary utilization method of nickel plating waste liquid, the method is to add 20-30% acid waste liquid recovery agent to the used acidic nickel plating waste liquid; or add 20% to the used alkaline nickel plating waste liquid -30% alkaline waste liquid recovery agent; rejuvenate the waste liquid and use it again as a new plating solution; the acidic waste liquid recovery agent is prepared by adding water to nickel sulfate, sodium hypophosphite, and sodium acetate; fully stir and mix during the preparation process Evenly filtered and mixed with nickel plating waste solution. During the preparation process, fully stir and mix evenly, filter and mix with nickel plating waste solution; check the pH value before mixing, and adjust the pH between 8 and 9 with ammonia water. The alkaline waste liquid recovery agent is prepared by adding nickel chloride, ammonium chloride, triammonium citrate, sodium hypophosphite and water. The acid waste liquid recovery agent is prepar...

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PUM

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Abstract

The invention discloses a secondary utilization method of nickel plating waste liquid. According to the secondary utilization method, 20 to 30% of an acidic waste liquid recycling agent is added into a used acidic nickel plating waste liquid, wherein the acidic waste liquid recycling agent is prepared from nickel sulfate, sodium hypophosphate, sodium acetate, and water; or 20 to 30% of an alkaline waste liquid recycling agent is added into a used alkaline nickel plating waste liquid, wherein the alkaline waste liquid recycling agent is prepared from nickel chloride, ammonium chloride, ammonium citrate tribasic, sodium hypophosphate, and water; so that the nickel plating waste liquid can be recycled, and can be used as plating liquid for a second time. According to the secondary utilization method, the nickel plating waste liquid is recycled by adding the waste liquid recycling agent, and abandoning of the used waste liquid residue is not necessary, so that resource waste is avoided, waste water treatment cost is reduced, and excellent beneficial effects are achieved.

Description

technical field [0001] The invention relates to a secondary utilization method of nickel plating waste liquid, belonging to the technical field of semiconductor nickel plating. Background technique [0002] In semiconductor production, it is necessary to plate nickel on the surface of the silicon wafer as a solder sintered between the die and the electrode in order to form a good ohmic contact with the silicon. There are generally two commonly used nickel plating methods, one is acid nickel plating, and the other is alkaline plating solution. [0003] At present, no matter whether acidic nickel plating or alkaline plating solution is used, the plating solution is only used once, and the remaining waste plating solution is poured out. These remaining waste plating solutions contain harmful substances, and cannot be directly discharged according to environmental protection requirements. For rivers and rivers, it takes a lot of manpower and material resources to process and me...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C18/36
Inventor 贺波刘态铭朱建凯杨辉
Owner CHINA ZHENHUA GRP YONGGUANG ELECTRONICS CO LTD STATE OWNED NO 873 FACTORY
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