A kind of antibacterial and deodorizing cellulose fiber and preparation method thereof

A cellulose fiber and fiber technology, applied in the field of antibacterial and deodorizing cellulose fiber and its preparation, can solve the problems of effective mineral loss and affecting the antibacterial and deodorizing functionality of finished fibers, etc., and achieve long-lasting effect and long-lasting and stable deodorizing function , wearing comfortable effect

Active Publication Date: 2016-01-13
QINGDAO JECELONG HIGH TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the above patents all belong to the use of natural aluminosilicate as a deodorizing adsorbent to prepare cellulose fibers, if the traditional cellulose fiber production process is adopted, as known knowledge, the pulp is soaked in lye and yellowed with carbon disulfide and then added with lye The viscose spinning solution is made into viscose spinning liquid, which is formed by wet spinning and spinning process after degassing and aging. The antibacterial and deodorizing function of the fiber, the test shows that after dissolving and adding aluminosilicate powder with a content of 7% p-methyl fiber, mixing evenly, spinning and refining, the burning residue method is used to detect the aluminum in the final fiber The content of silicate is about 1.9%, and more than 5% of the effective substances of aluminosilicate are decomposed and lost by sodium hydroxide and sulfuric acid

Method used

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  • A kind of antibacterial and deodorizing cellulose fiber and preparation method thereof
  • A kind of antibacterial and deodorizing cellulose fiber and preparation method thereof
  • A kind of antibacterial and deodorizing cellulose fiber and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Preparation of 0.78dtex×32mm antibacterial and deodorizing cellulose fibers:

[0034] (1) Preparation of bamboo charcoal nano-slurry

[0035] The preparation of bamboo charcoal nano-slurry is to add the bamboo charcoal powder with a particle size of 200~900 nanometers into 5.0wt% sodium hydroxide solution, stir for 45 minutes at a temperature of 41°C, add the dispersant dodecane after filtration Base benzene sulfonic acid, the quality that adds dispersant is 0.08wt% of bamboo charcoal nano-powder mass, after stirring 70 minutes under 800 rev / min rotating speeds, obtain the stable slurry that contains bamboo charcoal powder 35wt%, i.e. bamboo charcoal nano-powder.

[0036] (2) Preparation of aluminosilicate sustained-release microcapsules for use

[0037] The preparation of aluminosilicate sustained-release microcapsules includes:

[0038] (1) Pretreatment: Add natural aluminosilicate to 4.0wt% alkali solution, soak at 32°C for 35 minutes, wash at 41°C, filter and dry ...

Embodiment 2

[0047] Preparation of 1.11dtex×32mm antibacterial and deodorizing cellulose fibers:

[0048] (1) Preparation of bamboo charcoal nano-slurry

[0049] The preparation of bamboo charcoal nano-slurry is to add the bamboo charcoal powder with a particle size of 200~900 nanometers into 4.0wt% sodium hydroxide solution, stir at 40°C for 60 minutes, add dispersant into dodecylbenzenesulfonic acid after filtration , the adding quality of dispersing agent is 0.10wt% of bamboo charcoal nano-powder mass, after stirring 80 minutes under 500 revs / min rotating speed, obtain the stable slurry that contains bamboo charcoal powder 30wt%, i.e. bamboo charcoal nano-powder.

[0050] (2) Preparation of aluminosilicate sustained-release microcapsules for use

[0051] The preparation of aluminosilicate sustained-release microcapsules includes:

[0052] (1) Pretreatment: Add natural aluminosilicate to 3.0wt% alkali solution, soak at 30°C for 30 minutes, wash at 38°C, filter and dry at 77°C, then Al...

Embodiment 3

[0061] Preparation of 1.33dtex×38mm antibacterial and deodorizing cellulose fibers:

[0062] (1) Preparation of bamboo charcoal nano-slurry

[0063] The preparation of bamboo charcoal nano slurry is to add the bamboo charcoal powder with a particle size of 200~900 nanometers into 6.0wt% sodium hydroxide solution, stir at 43°C for 50 minutes, add the dispersant dodecylbenzenesulfonic acid after filtering, The mass of the dispersant added is 0.02wt% of the mass of the bamboo charcoal nano-powder, and after stirring for 60 minutes at a speed of 600 rpm, a stable slurry containing 40wt% of the bamboo charcoal powder is obtained, i.e. the bamboo charcoal nano-powder.

[0064] (2) Preparation of aluminosilicate sustained-release microcapsules for use

[0065] The preparation of aluminosilicate sustained-release microcapsules includes:

[0066] (1) Pretreatment: Add natural aluminosilicate to 5.0wt% alkali solution, soak at 34°C for 40 minutes, wash at 42°C, filter and dry at 83°C,...

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Abstract

The invention provides an antibacterial and deodorization cellulosic fiber which comprises 1-10wt% of aluminosilicate sustained-release microcapsule and 1-5wt% of bamboo charcoal nano powder, wherein the dry breaking strength of the antibacterial and deodorization cellulosic fiber is 1.80-2.60cN / dtex and the wet breaking strength is 0.90-1.50cN / dtex. A preparation method of the antibacterial and deodorization cellulosic fiber comprises preparation of denatured viscose, spinning and after-treatment, wherein the aluminosilicate sustained-release microcapsule is added in the processes of spinning and after-treatment. The antibacterial and deodorization cellulosic fiber has the advantages that the taking performance is excellent, the spinning performance is good and the antibacterial and deodorization functions are prominent; the bamboo charcoal sizing agent is dissolved and then is added into aluminosilicate powder, and then the bamboo charcoal sizing agent and the aluminosilicate powder are uniformly stirred, so that the aluminosilicate powder is prepared into the aluminosilicate sustained-release microcapsule; the aluminosilicate sustained-release microcapsule is added before the spinning by using a pre-spinning injection manner; in the presence of the microcapsule, the active substance decomposition loss and structure damage caused by the direct contact of the strong acid-base and aluminosilicate are prevented; along with the acid bath forming or friction fracture, the active ingredients of the aluminosilicate microcapsule in the textile are slowly released; the nano charcoal powder adsorbs the peculiar smell, so that the long-term antibacterial and deodorization functions are realized.

Description

technical field [0001] The invention relates to the technical field of modified cellulose, in particular to an antibacterial and deodorizing cellulose fiber and a preparation method thereof. Background technique [0002] With the progress of society and the improvement of people's living standards, the concept of people's clothing is constantly updated, which puts forward higher requirements for the functionality of textiles and the comfort and beauty of products. However, the production of natural fibers such as cotton, hemp, silk, and wool is affected by the natural climate and the contradiction between grain and cotton, and the output growth is very slow, which is far from meeting the actual demand. [0003] Cellulose in nature is not only a large reserve, but also an inexhaustible renewable resource. Only a very small part of this raw material is currently made into fibers. With the continuous deepening of human understanding of nature, the utilization of cellulose wil...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F2/08B01J13/02
Inventor 孙石林
Owner QINGDAO JECELONG HIGH TECH CO LTD
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