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A kind of manufacturing method of foamed microcrystalline material product by sintering method

A technology of microcrystalline materials and production methods, which is applied in the field of building materials, can solve the problems of controlling the crystallization process without description, etc., achieve good application prospects and practical value, increase strength, and be beneficial to environmental protection.

Inactive Publication Date: 2017-06-16
李嘉洋 +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Its process of controlling crystallization is not described

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0037] 60kg of gold mine tailings, 10kg of glass-ceramic frit water crushed material, 24kg of nepheline, 5kg of soda ash, and 1.0kg of silicon carbide are mixed and dry-milled until the particle size of the powder is ≤120 mesh. Fill these processed batch materials into refractory containers, and then heat them to 1160°C at a heating rate of 2-4°C / min in the kiln for 40 minutes of heat preservation and foaming; then heat them at a temperature of 10°C / min The temperature is lowered to 950°C at a cooling rate of 1°C / min, then to 550°C at a cooling rate of 1°C / min, and finally to room temperature at a cooling rate of 1-3°C / min.

[0038] The obtained product has an apparent density of 310g / m 3 , the compressive strength is 3.0Mpa, and the thermal conductivity is ≤0.10w / m.k. Finished products cut into standard sizes are packaged for storage.

example 2

[0040] 50kg of fly ash, 20kg of glass-ceramic frit water scrap, 25kg of quartz sand, 4kg of soda ash, and 1.0kg of silicon carbide are mixed and dry-milled until the particle size of the powder is ≤120 mesh. Fill these processed batch materials into refractory containers, and then heat them in the kiln to 1150°C at a heating rate of 2-4°C / min for foaming with heat preservation time of 40 minutes; Reduce the temperature to 950°C at a cooling rate of 1°C / min, then drop the temperature to 550°C at a cooling rate of 1°C / min, and finally drop the temperature to room temperature at a cooling rate of 1-3°C / min, and leave the furnace.

[0041] The obtained product has an apparent density of 230g / m 3 , the compressive strength is 2.0Mpa, and the thermal conductivity is ≤0.08w / m.k. Finished products cut into standard sizes are packaged for storage.

example 3

[0043] 50kg of coal gangue, 25kg of glass-ceramic frit water crushed material, 24kg of albite feldspar, and 1.0kg of silicon carbide are mixed and dry-milled until the particle size of the powder material is ≤120 mesh. Fill these processed batch materials into refractory containers, and then heat them in the kiln to 1170°C at a heating rate of 2-4°C / min. Reduce the temperature to 950°C at a cooling rate of 1°C / min, then drop the temperature to 550°C at a cooling rate of 1°C / min, and finally drop the temperature to room temperature at a cooling rate of 1-3°C / min, and leave the furnace.

[0044] The obtained product has an apparent density of 280g / m 3 , the compressive strength is 2.8Mpa, and the thermal conductivity is ≤0.09w / m.k. Finished products cut into standard sizes are packaged for storage.

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Abstract

The invention relates to a manufacturing method of a foamed microcrystalline material product by a sintering method. Its technical feature is that the raw material of foamed microcrystalline material products by sintering method is inorganic non-metallic solid waste as the main raw material, which is mixed with additional components such as microcrystalline glass frit water scrap containing crystal nucleating agent. In the production process, firstly, the mixture containing the crystal nucleating agent and foaming agent is prepared by means of mixed grinding, secondly, foaming is performed at high temperature during the firing process, and then the crystallization of the glass phase in the product is controlled by adjusting the cooling curve. The residual glass phase in the foamed microcrystalline material by the sintering method is greatly reduced, so that the material product has sufficient strength. The prepared sintered foamed microcrystalline material has the characteristics of light weight, heat insulation, sound absorption, high strength, etc., and can be widely used in the heat preservation needs of building walls and industrial equipment, and can realize industrial production.

Description

[0001] Technical field: [0002] The invention belongs to the field of building materials, and in particular relates to a method for manufacturing foamed microcrystalline material products by a sintering method by using inorganic non-metallic solid waste. [0003] Background technique: [0004] Due to the characteristics of non-combustibility and heat preservation, inorganic foamed microcrystalline materials have broad application prospects in the field of building energy conservation. [0005] Since the invention of this product, there have been a large number of open technologies and patented technologies for foamed glass, mainly using glass foaming to manufacture lightweight thermal insulation materials. The foaming process principle is the basis of the present invention, and the ceramic production process is the basis of the present invention. Base. [0006] The sintering method of foamed ceramics is usually a series of physical and chemical reactions of the ceramic batch ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C11/00C03C10/00
Inventor 李嘉洋刘鹏李晓明翟勇刘颖李佳
Owner 李嘉洋
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