Method for analyzing tracer substances in multi-stage fracturing fluid flowback fluid to evaluate fracturing effect
A technology of tracer substances and fracturing fluids, which is applied in the direction of earthwork drilling, production fluids, wellbore/well components, etc., can solve the problems of complex formation conditions, high cost, and many interference factors, and achieve intuitive and accurate fracturing conditions , Improve fracturing efficiency and reduce costs
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[0029] 1. Sampling: Take the fracturing flowback fluid directly from the sampling port of the oil well.
[0030] 2. Sample processing:
[0031] See figure 1 As shown, the fracturing fluid flowback fluid sample processing device of the present invention includes a digestion device 1 , an adsorption device 2 and a filtration device 3 connected in series through pipelines. Digestion device 1 is provided with sample inlet 11, H 2 o 2 Import, N 2 Through the inlet 12 and the air release port 13, a first valve 12 is provided on the pipeline between the digestion device 1 and the adsorption device 2, and a second valve 23 is provided on the pipeline between the adsorption device 2 and the filter device 3, and the filter The device 3 is provided with a filter membrane 31 of 0.45 μm, and is also provided with a liquid discharge port, and a third valve 33 is provided at the liquid discharge port, and the filter device is also equipped with a vacuum device (vacuum pump) 32 .
[0032...
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