Silicon Production with Fluidized Bed Reactor Utilizing Tetrachlorosilane to Reduce Wall Deposition
A fluidized bed reactor and reactor technology, applied in the direction of fluidized bed combustion equipment, silicon compounds, chemical instruments and methods, etc., can solve the problem that the product quality is not enough to be manufactured by integrated circuits
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[0034] A method of producing silicon comprising:
[0035] 1) supplying a deposition gas including hydrogen and silicon monomer to an inner region of a fluidized bed reactor (FBR), while
[0036] 2) supplying etching gas to the peripheral area of the FBR,
[0037] Wherein the peripheral area is located between the inner area and the FBR wall. In step 1), silicon monomers can be selected from silanes (SiH 4 ) and trichlorosilane (HSiCl 3 ). Deposition and etch gases are introduced into the heated zone of the FBR. The amount of silicon monomer in step 1) is sufficient to deposit silicon on the fluidized silicon particles in the reaction zone located above the heating zone of the FBR. The amount of etching gas in step 2) is sufficient to etch silicon on the walls of the FBR. The etching gas is basically composed of SiCl 4 composition.
[0038] In step 2) of the method, substantially SiCl 4 The composition etching gas is fed into the FBR and close to the FBR wall. Silic...
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