Preparing method for high-strength high-isolation condom comprising modified graphene/latex interlayer
A technology of graphene and condoms, applied in the direction of coating, etc., can solve the problems of easy falling off and damage, poor elasticity, high cost, etc., and achieve the effect of reducing and inhibiting the transmission probability and increasing comfort
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[0044] The preparation methods of modified graphene or graphene derivatives include but are not limited to the following three methods: ① Graphene powder or liquid dispersion prepared by expansion and exfoliation of graphite as raw material and subsequent modified products (fluorinated, (Carboxylation, sulfonation, amination, oxidation, grafting and other modification derivatives); ②graphene prepared by chemical vapor deposition (CVD) or physical vapor deposition (PVD) with gaseous carbon source as raw material and its subsequent modification (Fluorination, carboxylation, sulfonation, amination, oxidation, grafting and other modified derivatives); ③Powder or liquid phase formed by the aggregation of graphene-like two-dimensional sheet materials formed by chemical polymerization of small molecular substances Dispersion and its subsequent modification (fluorination, carboxylation, sulfonation, amination, oxidation, grafting, etc.).
[0045] The order of adding latex or pre-vulcaniz...
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[0057] Example 1
[0058] Add 200Kg of natural rubber latex with a concentration of 60wt% into a clean mixing tank, and gradually add 200Kg of sulfonated graphene aqueous solution with a concentration of 0.5wt‰ under stirring conditions. After the addition is complete, add 1wt%~ About 2wt% of dispersion stabilizer (such as sodium laurel silicate or F108), keep stirring for 1 hour to make it uniform. At this time, the viscosity is adjusted to about 15 mPa·s. The compounded glue is allowed to stand for about 24 hours to fully mature, and then perform three immersion production as described in the specific embodiment, and finally perform the performance test to obtain the finished product.
[0059] In order to verify the performance advantages of the new materials and condom products prepared by the present invention, the inventors used the national standard GB7544-2009 "Natural Latex Rubber Condom Technical Requirements and Experimental Methods" to compare the batches of graphene / ...
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[0069] Example 2
[0070] Add 200Kg of natural rubber latex with a concentration of 35wt% into a clean mixing tank, gradually add 200Kg of graphene oxide aqueous solution with a concentration of 0.05wt‰ under stirring conditions, and then add 0.5wt% to 1wt% respectively after adding. Dispersion stabilizer (such as sodium laurel silicate or F108), keep stirring for 1 hour to make it evenly mixed, and the viscosity is about 8mPa·s. The compounded glue is allowed to stand for about 24 hours to fully mature, and then added to the dipping machine for dipping production as described in the specific embodiment, and finally the finished product is obtained after passing the performance test.
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