Annular elastic ring for medical loop ligation device
A technology of elastic rings and ligation devices, applied in the field of annular elastic rings of medical ligation devices, can solve problems such as hindering the application and development of silicone rubber, poor mechanical strength, etc., to overcome poor mechanical strength, fast tissue shedding, and short ligation time Effect
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Embodiment 1
[0063] An annular elastic ring for a medical ligation device, including the following components in parts by mass: 100 parts of methyl vinyl silicone rubber, 2 parts of glycerin, 20 parts of precipitated white carbon black, and a coupling agent KH with a mass of 0.8% of white carbon black -560, 1 part of tert-butyl peroxybenzoate.
[0064] Its preparation method comprises the following steps:
[0065]Weigh the above raw materials according to the quality, and mix the medical grade methyl vinyl silicone rubber on the open mill; add precipitated silica, coupling agent KH-560 and glycerin in sequence, mix evenly, and the roller rotates at a low speed, controlled The roller temperature is below 40°C; the obtained product is thinly passed 4-8 times, and then placed in a 60°C oven for heat treatment for 12 hours. After the heat treatment of the silicone rubber, add 1 part of tert-butyl peroxybenzoate and knead evenly. The resulting product is thinly passed 5-8 times and parked over...
Embodiment 2
[0067] The annular elastic ring of the medical ligation device includes the following components in parts by mass: 100 parts of methyl vinyl phenyl silicone rubber, 5 parts of glycerin, 50 parts of precipitated white carbon black, and the mass is 2% of white carbon black. Agent Si69, 0.5 parts of di-tert-butyl peroxide.
[0068] Its preparation method comprises the following steps:
[0069] Weigh the above-mentioned raw materials according to the quality, and mix the medical grade methyl vinyl phenyl silicone rubber on an open mill; add precipitated silica, coupling agent Si69 and glycerin in sequence, first mix evenly on the open mill, roll The cylinder rotates at a low speed, and the temperature of the roller is controlled below 40°C. The obtained product is thinly passed 4-8 times, and then put into a 60°C oven for heat treatment for 12 hours. Add 0.5 parts of di-tert-butyl peroxide to the heat-treated silicone rubber, mix it evenly, pass through the product 5-8 times, and...
Embodiment 3
[0071] The annular elastic ring of the medical ligation device includes the following components in parts by mass: 100 parts of phenylene silicone rubber, 5 parts of glycerin, 30 parts of meteorological method hydrophilic white carbon black, and titanic acid with a mass of 1.5% white carbon black Ester coupling agent, 0.8 parts of dicumyl peroxide.
[0072] Its preparation method comprises the following steps:
[0073] Weigh the above raw materials according to the mass, and mix the medical grade phenylene silicone rubber on the open mill; add meteorological method hydrophilic white carbon black, titanate coupling agent and glycerin in sequence, and mix evenly on the open mill first , the roller rotates at a low speed, and the temperature of the roller is controlled below 40°C. The obtained product is thinly passed 4-8 times, and then put into a 60°C oven for heat treatment for 16 hours. After the heat treatment, add 0.8 parts of dicumyl peroxide and mix evenly for the heat-t...
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