A kind of Tongmai pharmaceutical composition and preparation method thereof
A technology for a composition and medicinal materials, applied in the field of medicine, can solve the problems of not being given, the composition is complex, etc., and achieve the effects of good drug efficacy, guaranteeing drug quality, and stable drug efficacy.
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Embodiment 1
[0065] Party:
[0066] Salvia 100g Chuanxiong 100g Pueraria Root 100g
[0067] Preparation:
[0068] Weigh the medicinal materials of Salvia miltiorrhiza, decoct once with 800g of water for 1 hour, and then use 500g of water for 2 times for half an hour; combine the decoctions, cool to room temperature, filter, and add ethanol to make the alcohol-containing The amount reaches 80%, refrigerate, filter, and concentrate the filtrate to a relative density of 1.10-1.15 at a temperature of 60 ° C. The obtained concentrate is injected into HPD600 type macroporous adsorption resin column, wherein the diameter-height ratio of the macroporous adsorption resin column is 1:6, the elution conditions are: the weight ratio of Dan to dry resin is 4:1, the adsorption flow rate is 3ml / min, and the elution flow rate is 4ml / min. Then use 8 times the column volume of 20% ethanol to elute, discard the eluent, and then use 6 times the column volume of 75% ethanol to elute, and collect the 75% etha...
Embodiment 2
[0073] Party:
[0074] Salvia 100g Chuanxiong 100g Pueraria Root 100g
[0075] Preparation:
[0076] Weigh the medicinal materials of Salvia miltiorrhiza, decoct once with 800g of water for 1 hour, and then use 500g of water for 2 times for half an hour; combine the decoctions, cool to room temperature, filter, and add ethanol to make the alcohol-containing The amount reaches 80%, refrigerate, filter, and concentrate the filtrate to a relative density of 1.10-1.15 at a temperature of 60 ° C. The obtained concentrate is injected into HPD600 type macroporous adsorption resin column, wherein the diameter-height ratio of the macroporous adsorption resin column is 1:7, the elution conditions are: the weight ratio of Dan to dry resin is 4:1, the adsorption flow rate is 3ml / min, and the elution flow rate is 4ml / min; during elution, 8 times the column volume of purified water is used to elute, Then use 8 times the column volume of 20% ethanol to elute, discard the eluent, and then u...
Embodiment 3
[0081] Party:
[0082] Salvia 100g Chuanxiong 100g Pueraria Root 100g
[0083] Preparation:
[0084] Weigh the medicinal materials of Salvia miltiorrhiza, decoct once with 800g of water for 1 hour, and then use 500g of water for 2 times for half an hour; combine the decoctions, cool to room temperature, filter, and add ethanol to make the alcohol-containing The amount reaches 80%, refrigerate, filter, and concentrate the filtrate to a relative density of 1.10-1.15 at a temperature of 60 ° C. The obtained concentrate is injected into HPD600 type macroporous adsorption resin column, wherein the diameter-height ratio of the macroporous adsorption resin column is 1:8, the elution conditions are: the weight ratio of Dan to dry resin is 4:1, the adsorption flow rate is 3ml / min, and the elution flow rate is 4ml / min. Then use 8 times the column volume of 20% ethanol to elute, discard the eluent, and then use 6 times the column volume of 75% ethanol to elute, and collect the 75% ethano...
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