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A kind of deep processing preparation and quality control method of propolis compound

A technology of propolis extract and propolis, which is applied in the field of deep processing and preparation of propolis products, can solve problems such as poor properties of propolis powder, unqualified products, and difficulty in drying, so as to improve dissolution and disintegration time, improve product curative effect, improve The effect of product quality

Active Publication Date: 2019-11-12
BY HEALTH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] After propolis is extracted and concentrated by ethanol, the obtained extract is very viscous and is usually difficult to dry. In order to make the extract dry smoothly, it is necessary to add auxiliary materials to it, such as starch, maltodextrin, lactose, etc., but because the propolis extract contains There are also a large amount of tannin components such as gums and resins, which are relatively weak in polarity and bonded into agglomerates, which often cannot be mixed evenly with auxiliary materials, and then a uniform system cannot be obtained for the next drying process, resulting in poor powder properties of propolis powder. Poor, it cannot be uniformly mixed with other raw materials of the product formula, which ultimately affects the product preparation process; at the same time, because propolis contains a large number of compounds with aldehydes, ketones, phenolic hydroxyl groups, etc. The amine groups of gelatin will undergo condensation and cross-linking reactions with each other, resulting in the disintegration of propolis powder prepared by traditional techniques after being made into tablets, hard capsules, and soft capsules during the shelf life. A problem with the requirement that results in the product being judged as non-conforming

Method used

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  • A kind of deep processing preparation and quality control method of propolis compound
  • A kind of deep processing preparation and quality control method of propolis compound
  • A kind of deep processing preparation and quality control method of propolis compound

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preparation example Construction

[0042] The invention discloses a preparation method of propolis powder and a product thereof. Those skilled in the art can refer to the content of this article and appropriately improve the process parameters to realize it. In particular, it should be pointed out that all similar replacements and modifications are obvious to those skilled in the art, and they are all considered to be included in the present invention. The method and application of the present invention have been described through preferred embodiments, and the relevant personnel can obviously make changes or appropriate changes and combinations to the method and application described herein without departing from the content, spirit and scope of the present invention to realize and Apply the technology of the present invention.

[0043] The preparation method of the propolis powder provided by the invention and the raw materials or auxiliary materials used in the product can be purchased from the market.

Embodiment 1

[0045] The preparation of embodiment 1 propolis powder

[0046] 1. Pretreatment

[0047] Freezing the raw material of Brazilian green propolis at -20°C for 3 hours to harden the propolis; then crushing it with a pulverizer to obtain the raw material of propolis powder;

[0048] 2. Extraction

[0049] Take the pulverized propolis raw material, put it in an extraction tank, add 85% ethanol in an amount 4 times the volume of the medicinal material, stir and extract at room temperature for 3 hours, filter, and store the filtrate separately; add 4 times the amount of 85% ethanol to extract with stirring at room temperature for 3 hours, filter , take the filtrate, and combine the extracts.

[0050] 3. Concentration and grinding

[0051]Test group: take the propolis ethanol extract and concentrate it in a concentrator under reduced pressure. The vacuum degree is controlled at -0.01MPa and the temperature is 50°C. Centrifuge at a speed of 2000r / min for 5min, remove the suspended m...

Embodiment 2

[0061] The preparation of embodiment 2 propolis powder

[0062] 1. Pretreatment

[0063] Freezing the raw material of Brazilian green propolis at -20°C for 3 hours to harden the propolis; then crushing it with a pulverizer to obtain the raw material of propolis powder;

[0064] 2. Extraction

[0065] Take the pulverized propolis raw material, put it in an extraction tank, add 75% ethanol in an amount 10 times the volume of the medicinal material, stir and extract at room temperature for 2 hours, filter, and store the filtrate separately; , take the filtrate, and combine the extracts.

[0066] 3. Concentration and grinding

[0067] Test group: take the propolis ethanol extract and concentrate it in a concentrator under reduced pressure. The vacuum degree is controlled at -0.03MPa and the temperature is 60°C. Centrifuge at a speed of 1500r / min for 8min, remove the suspended matter in the upper layer, and then take the centrifuged liquid and continue to concentrate under redu...

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Abstract

The invention relates to a processing field of a propolis product, and particularly relates to a deep processing preparation method of the propolis powder and its product. The propolis composite is prepared by hardening and crushing the propolis raw material, and obtaining the propolis raw material powder; performing alcohol extraction on the propolis raw material powder, and obtaining the thick paste of the propolis extractive; mixing the propolis extractive thick paste with amino acid; grinding, cooling and drying, crushing and obtaining the propolis powder. The preparation method adds amino acid to the propolis extractive thick paste, thus the propolis and the amino acid can form an uniform system, thus the propolis can be smoothly dried, and the propolis powder with good powder property is obtained; meanwhile, the propolis powder prepared by the process is applicable to the propolis capsule (including hard capsule and soft capsule), propolis slice and others; the method can significantly improve the collapse problem of the propolis product.

Description

technical field [0001] The invention relates to the field of propolis processing, in particular to a preparation method for deep processing of propolis products and products thereof. Background technique [0002] Propolis is a colloidal solid with an aromatic smell that is processed by bees from the resin collected from plant spores or tree trunks and mixed with the secretions of their palate glands and wax glands. It is a yellow-brown or dark-brown viscous substance secreted by Apis mellifera and other animals repairing the hive, which can be used as medicine. It is flat in nature, bitter, pungent, and slightly sweet. It has the effects of moisturizing skin and promoting muscle growth, reducing inflammation and relieving pain, and can treat gastric ulcers, oral ulcers, burns, skin cracks, and radiation protection. Over the years, it has been mainly used clinically for capillary hemostatic drugs and auxiliary antihypertensive drugs. In addition to flavonoids, propolis also...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K35/644A61K47/18A61P39/06A61P37/04G01N9/00G01N15/00
CPCA61K35/644A61K47/18G01N9/00G01N15/00
Inventor 何健黄远英殷光玲张铭辉
Owner BY HEALTH CO LTD
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