Preparation method of magnetic chitosan carbon spheres and application thereof in adsorbing and removing Cr (VI) in water
A chitosan and water removal technology is applied in the preparation of magnetic chitosan carbon spheres, and the magnetic chitosan carbon spheres remove Cr from water, which can solve the problems of complicated preparation process, decreased adsorption performance, and a large amount of organic solvents, and achieves Simple process, easy operation, strong physical and chemical stability
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Embodiment 1
[0040] 1. Preparation of magnetic cobalt ferrite
[0041] (1) Weigh 2.71g FeCl respectively 3 ·6H 2 O and 1.19 g CoCl 2 ·6H 2 O was dissolved in 50 mL of distilled water;
[0042](2) under magnetic stirring, in the solution obtained by step (1), add dropwise 2mol / L sodium hydroxide solution to pH greater than 11, transfer the solution to a 100mL hydrothermal reaction kettle (filling degree≤75%), Place in a high-temperature furnace for 180°C hydrothermal reaction for 24 hours;
[0043] (3) After natural cooling, the solid-liquid obtained in step (2) is magnetically separated, and the obtained solid is repeatedly washed with 0.1mol / L HCl and distilled water until neutral, dried at 60°C, ground and sieved to obtain magnetic cobalt ferrite .
[0044] 2. Preparation of magnetic chitosan carbon spheres
[0045] (1) Weigh chitosan and cobalt ferrite according to the mass ratio of chitosan and magnetic cobalt ferrite being 1:1, add 50mL of distilled water and ultrasonically dis...
Embodiment 2
[0049] 1. Preparation of magnetic cobalt ferrite
[0050] With embodiment 1.
[0051] 2. Preparation of magnetic chitosan carbon spheres
[0052] With embodiment 1, the difference is that the mass ratio of adding chitosan and magnetic cobalt ferrite is 2:1.
Embodiment 3
[0054] 1. Preparation of magnetic cobalt ferrite
[0055] With embodiment 1.
[0056] 2. Preparation of magnetic chitosan carbon spheres
[0057] With embodiment 1, difference is to add chitosan and magnetic cobalt ferrite mass ratio is 3:1.
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