Use of a composition containing 1,3-propanediol as an e-liquid
A technology of propylene glycol and composition, applied in the field of electronic cigarettes
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example 2
[0066] Example 2 : Formulation and analysis of PDO-based compositions
[0067] Proceed in the same manner as Example 1, but replace the plant-derived propylene glycol with 1,3-propanediol manufactured by DuPont&Tate&Lyle LLC under Cat. No. Provided by Propanediol.
[0068] result :
[0069] Under the analytical conditions (sensitivity 0.5 ng / g), no trace of propylene oxide was detected, nor traces of dipropylene glycol and tripropylene glycol.
[0070] The biogenic carbon content of the mixture is equal to 99.7%.
[0071] (Contrast) Example 3 : Formulation and Analysis of Synthetic Propylene Glycol Based Compositions
[0072] Proceed in the same manner as Example 1, but replace the plant-derived propylene glycol with synthetic propylene glycol, manufactured by Dow under Cat. No. Provided by Propylene glycol, USP grade.
[0073] result :
[0074] Under the analytical conditions (sensitivity 0.5 ng / g), no traces of dipropylene glycol and tripropylene glycol wer...
example 4
[0077] Example 4 : Formulation and analysis of glycerol-free compositions
[0078] Proceed in the same manner as Example 1, but replace plant-derived glycerol and propylene glycol with plant-derived PDO according to Example 2.
[0079] result :
[0080] Under the analytical conditions (sensitivity 0.5 ng / g), no trace of propylene oxide was detected, nor traces of dipropylene glycol and tripropylene glycol.
[0081] The biogenic carbon content of the mixture is equal to 99.8%.
example 5
[0082] Example 5 : Assessing the efficacy of different e-liquids
[0083] By providing a trademarked And the model is eCab TM (December 2013 model) panel of 10 smokers to evaluate the e-liquid compositions formulated in Examples 1 to 4. Each reservoir is filled with an equal amount of e-liquid (1ml).
[0084] In this way, each group member inhales 8 times continuously every 20 seconds according to the blind test method, and there is a heating time of 2 seconds before each inhalation. Evaluations are based on scoring on a scale of 1 to 10 for vapor density criteria and perceived aroma intensity criteria. Each panelist transitioned from one product to another as follows: 5 minutes after the last inhalation, the panelist rinsed with 2 glasses of 100 ml of water and then drank 50 ml of water. There was a 10-minute break between each assessment.
[0085] The average results obtained are compiled in the table below:
[0086]
[0087] Apparently, plant-derived propylene g...
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