Method for judging doubtful values of sample detection data

A technology for detecting data and samples, which is applied in the field of judging the suspicious value of sample detection data, and can solve the problems of reducing the accuracy and reliability of the detection data, and the abnormal data cannot be found and eliminated.

Inactive Publication Date: 2017-04-05
PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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Problems solved by technology

[0002] Usually, the methods and rules of mathematical statistics are used in the statistical analysis of sample detection data, such as Grubbs test, Dixon test, etc. There are often blind spots in the Sidney test and the Dixon test. In the case of non-normal distribution (that is, there are extreme values), some abnormal data cannot be found and eliminated, which reduces the accuracy and reliability of the test data.

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  • Method for judging doubtful values of sample detection data
  • Method for judging doubtful values of sample detection data
  • Method for judging doubtful values of sample detection data

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[0022] Such as figure 1 The method for judging the suspicious value of sample detection data in the present invention includes:

[0023] A. The detection data of the same element in the same sample in P laboratories are measured n times respectively to form P sets of data, each set of data has n values, where P and n are respectively integers ≥ 1, this implementation In the example n is 4;

[0024] B. Through the intragroup repeatability variance s of each group of data r 2 Computes the within-group repeatability value r.

[0025] within-group repeatability variance Among them, P is the number of laboratory groups participating in the calculation. When a laboratory is discarded, P is the number of remaining laboratory groups, n i is the number of determinations of the i laboratory n=4, s i 2 It is the square of the standard deviation of the measurement results of the i laboratory; the repeatability value within the group r=2.8×s r ,in

[0026] C. Calculate the rang...

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Abstract

The invention relates to a method for judging doubtful values of sample detection data. The method comprises the following steps of: A, respectively carrying out n tests on detection data of same elements of same samples in P laboratories; B, calculating an intragroup repeatability value r; C, if the range of n numerical values of the ith laboratory is greater than or equal to the repeatability value r, retesting or abandoning the laboratory, and otherwise, indicating that the laboratory passes repeatability judgement; D, repeating the steps B to C, and re-calculating the repeatability value r until the residual laboratories pass the repeatability judgement; E, if the range of the average value of the laboratories which pass the repeatability judgement is greater than or equal to a reproducibility value R, retesting or abandoning the test numerical values of two corresponding laboratories; and F, considering the residual test numerical values as qualified numerical values. According to the method provided by the invention, the dead zones of common Grubbs test and Dixon doubtful value test are overcome, more scientific judgement is carried out on data during constant value analysis, and beneficial supplementation is carried out on the traditional guide sample development data statistical analysis method.

Description

technical field [0001] The invention relates to a method for analyzing standard sample data, in particular to a method for judging suspicious values ​​of sample detection data. Background technique [0002] Usually, the methods and rules of mathematical statistics are used in the statistical analysis of sample detection data, such as Grubbs test, Dixon test, etc. There are often blind spots in the Sidney test and Dixon test. In the case of non-normal distribution (that is, there are extreme values), some abnormal data cannot be found and eliminated, which reduces the accuracy and reliability of the detection data. The Chinese invention patent "Method for Judging Suspicious Value of Sample Test Data" (ZL201410088717.6) is based on Robust statistics, using the median value and standard interquartile range to analyze and judge the test data. In addition, other judging methods can also be established to judge the data from different angles when analyzing the fixed value. Cont...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G06F19/00
CPCG16Z99/00
Inventor 徐本平
Owner PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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