Method for identifying producing area of Wuyi rock tea through combination of near infrared spectroscopy and trace element detection

A technology of near-infrared spectroscopy and trace elements, which is applied in the field of identification of the origin of Wuyi rock tea, can solve the problem that the detection data cannot represent all the key information of the traceability of the origin

Inactive Publication Date: 2017-04-12
CHINA JILIANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The purpose of the present invention is to solve the problem that a single detection data cannot represent all the key information of origin traceability, and also solve the problems of joint use of different types of detection data in metrology methods, analysis of existing data matching, etc., and provide a combined near-infrared Wuyi rock tea origin identification model technology method based on spectral data and trace element data. This method is based on the least squares support vector machine discriminant model, and combines the near-infrared characteristic spectral data and trace element data of rock tea within and outside the origin of the geographical indication. , establish an analysis model, and use the model to objectively and accurately determine the origin of rock tea after extracting samples

Method used

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  • Method for identifying producing area of Wuyi rock tea through combination of near infrared spectroscopy and trace element detection
  • Method for identifying producing area of Wuyi rock tea through combination of near infrared spectroscopy and trace element detection
  • Method for identifying producing area of Wuyi rock tea through combination of near infrared spectroscopy and trace element detection

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Effect test

Embodiment 1

[0077] A. Collect rock tea samples from different origins

[0078] The national standard (GB / T 18745-2006) stipulates the scope of geographical protection of Wuyi rock tea, that is, within the administrative division of Wuyishan City, Fujian Province, the present invention is located in Wuyi Street, Chong'an Street, Shangmei, and Xingxia in the Wuyi Rock Tea Geographical Indication Protection Area. Samples were collected in 11 administrative areas including Village, Wufu, Langu, Xinfeng Street, Yangzhuang, Xingtian, Xiamei, and Wutun, and 3 sampling points were randomly selected in each administrative area (respectively A, B, C to be marked), a total of 33 sampling points, the sampling range basically covers the main production areas, and each sampling point takes 15 samples (respectively marked with A-1, A-2...A-15), and obtained 495 samples of Wuyi rock tea in geographical indication protected areas, and other counties and cities in Fujian Province except Wuyishan City (Jian...

Embodiment 2

[0124] Blind sample detection: The blind sample supervision team purchases rock tea samples from Wuyi rock tea farmers, monitors the steps of drying, greening, and finishing to ensure the origin of the rock tea samples. The above samples are used as geographical indications in the blind samples. Samples in the region; rock tea was purchased from Jianyang, Jianou, Wuyuan and other places as samples outside the geographical indication production area in the blind sample. The above blind sample and the modeling rock tea sample came from different manufacturers. Analyzing and testing personnel failed to know the origin attribute of the blind sample to be tested in advance, randomly selected several copies, tested, and then judged the origin attribute of the blind sample according to the method of the present invention, and checked with the blind sample supervision team to determine the recognition rate of the blind sample . 20, 60, and 100 blind samples were selected respectively,...

Embodiment 3

[0126] Using the same modeling data as in Example 1, the data segmentation uses the Duplex segmentation program, and uses the K-fold interactive verification to set up the least squares support vector machine (LS-SVM) model, neural network ELM and partial least squares (PLSDA) respectively. ) model, the near-infrared spectrum data remains unchanged, and the trace element data are spliced ​​after the near-infrared data in the order of Cs, Cu, Ca, Rb, Sr, Ba, Mg, Mn, Ti, Cr, Co, Ni, Zn, and Cd. The recognition rates of the models are 91.3%, 87.8%, and 89.5%, respectively.

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Abstract

The invention relates to a method for identifying the producing area of Wuyi rock tea through a combination of near infrared spectroscopy and trace element detection, belonging to the technical field of identification of the authenticity of products of geographical indication. The objective of the invention is to overcome the problems that single detection data cannot represent all the key information in tracing of a producing area and that data matching is hard to realize for combined usage of detection data of different types in metrological method and other problems in the prior art. According to the invention, near-infrared characteristic spectroscopic data and trace element data of rock tea from different producing areas (including rock tea from and not from a geographically indicated producing area) are fused together for establishing a least squares support vector machine (LS-SVM) analysis model on the basis of a LS-SVM model, and the model is used for objectively and accurately determining the producing area of an extracted sample; the method has the highest identification rate, as high as 100.0% and much higher than LS-SVM determination results composed of single near-infrared or trace element data; and the method has a blind sample identification rate of 100%, so the method has good application prospects.

Description

[0001] (1) Technical field [0002] The invention relates to a method for identifying the origin of Wuyi rock tea by combining near-infrared spectroscopy and trace elements, and belongs to the technical field of authenticity identification of geographical indication products. [0003] (2) Background technology [0004] Geographical indication products refer to products whose quality, reputation or other characteristics are essentially determined by the natural and human factors of the place of origin, and which are named after examination and approval with geographical names. Tea is a typical geographical indication protected product, and its quality and taste are closely related to the geographical conditions, climate factors, environment and other factors of the place of origin. Wuyi rock tea is one of the representative tea products. [0005] At present, domestic and foreign finished tea origin identification methods are based on single instrument detection and analysis comb...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/359
CPCG01N21/359
Inventor 叶子弘楼云霄付贤树俞晓平崔海峰张雅芬
Owner CHINA JILIANG UNIV
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