Method for preparing graphene modified polyimide-based composite film and flexible printed circuit board
A polyimide film, graphene modification technology, applied in the direction of circuit substrate materials, printed circuits, printed circuits, etc., can solve the problems of inability to accurately control the thickness, low thickness uniformity, high production cost, and achieve superior processing performance. , low cost, improve the effect of trial life
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[0030] A kind of preparation method of graphene modified polyimide composite film, comprises the following steps:
[0031] a. Graphene preparation:
[0032] a1 Add graphite to the pre-configured strong oxidation system of nitric acid and concentrated sulfuric acid, and react for a period of time to obtain graphite oxide solution;
[0033] a2, add NaNO in the graphite oxide solution in step a1 3 After stirring, add potassium permanganate to reduce graphite oxide;
[0034] a3, after the solution in step a2 is ultrasonically treated, the graphene is obtained by centrifugal washing and drying;
[0035] b, also prepared on foot: dissolving the polyimide in a polar solvent, and adding the graphene obtained in step a and stirring to obtain a graphene-modified polyimide solution;
[0036] c. Coating and film formation: Coating the graphene-modified polyimide solution in step b on the polyimide film by coating and drying;
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