A kind of compound and its salt and synthesis method thereof
A technology of compounds and thiol compounds, which is applied in the field of compounds and their salts and their synthesis, can solve the problem that there is no preparation method for 3-mercaptomethylindole compounds
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Embodiment 1-35
[0066] Step 1: Add indole compounds (see Table 1 for specific substances) and thiophenol compounds (see Table 1 for specific substances) into the reaction vessel, and add the Lewis base (see Table 1 for specific substances) solution into the reaction vessel. Add Lewis base (see Table 1 for specific substances) and distilled water in the container;
[0067] Step 2: Heat the reaction vessel uniformly (such as heating in a water bath) to the temperature described in Table 1. Indole compounds and thiophenol compounds float on the water phase to cause an organic reaction on water, and continue in Table 1. Said time
[0068] Step 3: Purification.
[0069] In the reaction of the above embodiment, the Lewis base depolymerizes the paraformaldehyde and connects the indole compound and the thiophenol compound to finally generate the desired compound. The raw materials of the above preparation method are all easily obtainable chemical products, the reaction conditions are simple, and the purif...
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