An eight immortal flower leaf extract and its drug composition, preparation method and application
A technology of leaf extract and hydrangea, applied in the field of preparation, hydrangea leaf extract and pharmaceutical compositions thereof, can solve problems such as the production process blank of total phenolic acid extract of hydrangea, and achieve stable and controllable quality and economical process. , the effect of clear treatment effect
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Embodiment 1
[0033] Example 1 Preparation of total phenolic acid extract of hydrangea flower leaves (1)
[0034] The dried medicinal materials of 2kg of pulverized hydrangea leaves were added in 60% ethanol for 12 hours in a ratio of 1:5 by weight of the medicinal materials: ethanol solution, and then heated and refluxed for 3 times, each extraction time was 2h, 2h, 2h. Combine the three extracts, filter, recover the solvent, and concentrate to a relative density of 1.00-1.20. The concentrated liquid was extracted three times with petroleum ether and n-butanol respectively, and extracted according to the ratio of concentrated liquid: solvent weight ratio of 1:1. The three n-butanol extracts were combined and concentrated to obtain 67.8 g of the n-butanol extract. The n-butanol extract was dissolved in 1.5L of distilled water, filtered, and the filtrate was adsorbed on a 2kg AB-8 type macroporous resin column, and the adsorption was repeated three times. First, use 3 times the column volume...
Embodiment 2
[0035] Example 2 Preparation of total phenolic acid extract of hydrangea flower leaves (2)
[0036] 2kg of the dried medicinal materials of the pulverized hydrangea leaves were added with 70% ethanol at a weight ratio of 1:10, soaked in 70% ethanol for 12 hours, and then heated and refluxed for 3 times, each extraction time was 2h, 2h , 2h. Combine the three extracts, filter, recover the solvent, and concentrate to a relative density of 1.00-1.20. The concentrated liquid was extracted three times with petroleum ether and n-butanol respectively, and the concentrated liquid: solvent weight ratio was 1:1. The three n-butanol extracts were combined and concentrated to obtain 85.3 g of the n-butanol extract. The n-butanol extract was dissolved in 2.8L of distilled water, filtered, and the filtrate was adsorbed on a 4kg HPD300 type macroporous resin column, and the adsorption was repeated three times. For the first time, use 4 times the column volume of distilled water and 5 times t...
Embodiment 3
[0037] Example 3 Preparation of total phenolic acid extract of hydrangea flower leaves (3)
[0038] The dried medicinal materials of 2kg of pulverized hydrangea leaves were added with 90% ethanol at a weight ratio of 1:20 in the ratio of medicinal materials: ethanol solution for 24 hours, and then heated and refluxed for 3 times, each extraction time was 3h, 3h , 3h. Combine the three extracts, filter, recover the solvent, and concentrate to a relative density of 1.00-1.20. The concentrated liquid was extracted three times with petroleum ether and n-butanol respectively, and the concentrated liquid: solvent weight ratio was 1:1. The three n-butanol extracts were combined and concentrated to obtain 167 g of n-butanol extract. The n-butanol extract was dissolved in 2.0L of distilled water, filtered, and the filtrate was adsorbed on a 3kg D101 macroporous resin column, and the adsorption was repeated three times. For the first time, use 6 times the column volume of distilled wate...
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