Breathable infant toilet powder and preparation method thereof
A talcum powder, infant technology, applied in the field of baby skin care products, can solve the problems of skin sweat gland blockage, unsafe physical development of infants, breeding bacteria, etc., to achieve the effect of avoiding clogged pores, keeping the skin dry, and good respiratory protection
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Embodiment 1
[0032] A kind of preparation method of baby's talcum powder that can breathe, comprises the following steps:
[0033] (1) After cleaning the honeysuckle, Radix isatidis, chrysanthemum, and shoot dry, add 2 times of water, raise the temperature to 80°C at a rate of 5°C / min, then keep warm for 30 minutes, then add 1 times of water, and continue to keep warm for 1 hour to get Chinese medicine mixture, filtering the Chinese medicine mixture to obtain medicinal liquid and medicinal residues;
[0034] Continue decocting the medicinal dregs for 2 times according to the above method, and combine the filtrate obtained three times to obtain the Chinese medicine extract;
[0035] (2) The Chinese medicine extract is reacted with methyltrimethoxysilane in ethyl acetate to form a precursor;
[0036](3) Add 1 volume of methanol to the precursor solution, stir for 1 minute, separate the organic layer, then put it into a spray dryer, and spray the precursor solution under reduced pressure at ...
Embodiment 2
[0039] A kind of preparation method of baby's talcum powder that can breathe, comprises the following steps:
[0040] (1) After cleaning the honeysuckle, isatis root, chrysanthemum, and shoot dry, add 2 times the water, raise the temperature to 80 ℃ at a rate of 5 ℃ / min, and keep warm for 30 minutes, then add 2 times the water, and continue to keep warm for 3 hours to get Chinese medicine mixture, filtering the Chinese medicine mixture to obtain medicinal liquid and medicinal residues;
[0041] Continue decocting the medicinal dregs for 2 times according to the above method, and combine the filtrate obtained three times to obtain the Chinese medicine extract;
[0042] (2) The Chinese medicine extract is reacted with methyltrimethoxysilane in ethyl acetate to form a precursor;
[0043] (3) Add 2 times the volume of methanol to the precursor solution, stir for 20 minutes, separate the organic layer, then put it into a spray dryer, and spray dry the precursor solution under redu...
Embodiment 3
[0046] A kind of preparation method of baby's talcum powder that can breathe, comprises the following steps:
[0047] (1) After cleaning the honeysuckle, Radix isatidis, chrysanthemum, and shoot dry, add 2 times the water, raise the temperature to 85 ℃ at a rate of 7 ℃ / min, and keep warm for 45 minutes, then add 2 times the water, and continue to keep warm for 2 hours to get Chinese medicine mixture, filtering the Chinese medicine mixture to obtain medicinal liquid and medicinal residues;
[0048] Continue decocting the medicinal dregs for 2 times according to the above method, and combine the filtrate obtained three times to obtain the Chinese medicine extract;
[0049] (2) React the Chinese medicine extract with ethyltrimethoxysilane in dichloromethane to form a precursor;
[0050] (3) Add 3 times the volume of ethanol to the precursor solution, stir for 60 minutes, separate the organic layer, then put it into a spray dryer, and spray dry the precursor solution under reduce...
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