The invention relates to the technical field of
copper alloy preparation, in particular to a preparation method of high-density low-free-
oxygen-content dispersed
copper, which comprises the following steps: preparing
copper-aluminum
powder through atomization
powder preparation, carrying out
internal oxidation and reduction by using the oxidized
powder of the copper-aluminum powder as an
oxygen source to obtain aluminum
oxide / copper powder, filling the aluminum
oxide / copper powder into a steel
ladle sleeve, vacuumizing, introducing
hydrogen, and carrying out high-density low-free-
oxygen-content dispersed copper. Aluminum
oxide / copper powder is subjected to on-line reduction at a high temperature, a powder
ingot with low free oxygen is obtained after high-temperature hot degassing, and then
hot isostatic pressing and hot
extrusion are performed to obtain the dispersion copper with
high density and low free
oxygen content. The
relative density of the obtained dispersion copper is larger than or equal to 98%, and the free
oxygen content is smaller than or equal to 20 ppm. According to the method, a
solid reducing agent is not introduced, external elements are not introduced, the high-density and low-free-oxygen-content dispersed copper is obtained through
hydrogen online reduction, and the use requirement of a
divertor is met.