The invention discloses a comprehensive
recovery method of
nickel-
cobalt-containing matte, and relates to the technical field of non-
ferrous metal metallurgy, and the method comprises the following steps: step 1, oxidation blowing: adding
nickel-
cobalt-containing matte into an
oxidation zone of a double-zone converting furnace, adding a mixed flux, blowing high-speed
oxygen flow by a top-blowing spray gun, and controlling the flux rate to be 3-5% to obtain crude
copper and blowing
slag floating on the upper layer; the converting
slag overflows into a reduction area through the upper portion of the partition wall,
oxygen-enriched air, fuel and a vulcanizing agent are blown in through a side-blowing spray gun, the
mass ratio of the vulcanizing agent to the hot
slag is controlled to be 20-30%, the
coal rate is controlled to be 3-5%, the
oxygen concentration is controlled to be 25-40%, the volume ratio of CO / (CO + CO2) in
smoke is controlled to be 40-70%, and after
smelting is conducted for 2.5-3 h, high-
nickel-
cobalt matte and reducing slag are obtained. According to the method, the nickel and cobalt elements in the converting slag are directly enriched into the high-nickel-cobalt matte in the same
smelting device, the problem that the Ni and Co elements are circularly enriched in the
system along with the slag is solved, and meanwhile comprehensive
recovery of the Ni and Co elements is achieved.