A kind of fish pesticide and preparation method thereof
An insecticide and fishery technology, applied in the field of fishery insecticide and its preparation, can solve problems such as drug residues in aquatic products, ecological safety hazards of farmed animals, drug resistance of pathogens, etc., and achieve fast adsorption rate and shorten Response time, the effect of not easy to fall off
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Embodiment 1
[0024] An insecticide for fishing, comprising a main drug part and an auxiliary drug part, the main drug part is prepared by adsorbing furfural with ligninyl glycyrrhetinic acid gel, and the auxiliary drug part contains the following components in weight percentage: Buds subtilis Bacillus subtilis bacteria liquid 45%, onion 25%, oleander 10%, Tween 2.0%, glutathione 0.1%, and the balance is water.
[0025] The preparation method of above-mentioned fish insecticide comprises the following steps:
[0026] (1) Preparation of glycyrrhetinic acid succinate: 4.7g (10.0mmol) glycyrrhetinic acid was dissolved in 80ml of N,N-dimethylformamide, followed by adding 1.3g (10.0mmol) anhydrous potassium carbonate , 4.5g (45.0mmol) succinic anhydride and 1ml catalyst (prepared from pyridine and N,N-diisopropylethylamine at a volume ratio of 1:5), reacted in a dark room at 50°C for 6h, and cooled to At room temperature, add a large amount of water, then add ethyl acetate to extract, take the ...
Embodiment 2
[0031] An insecticide for fishing, comprising a main drug part and an auxiliary drug part, the main drug part is prepared by adsorbing furfural with ligninyl glycyrrhetinic acid gel, and the auxiliary drug part contains the following components in weight percentage: Buds subtilis Bacillus subtilis bacteria liquid 50%, onion 30%, oleander 15%, Tween 3.0%, glutathione 0.3%, and the balance is water.
[0032] The preparation method of above-mentioned fish insecticide comprises the following steps:
[0033] (1) Preparation of glycyrrhetinic acid succinate: 4.7g (10.0mmol) glycyrrhetinic acid was dissolved in 80ml of N,N-dimethylformamide, followed by adding 1.3g (10.0mmol) anhydrous potassium carbonate , 4.5g (45.0mmol) succinic anhydride and 1ml catalyst (prepared from pyridine and N,N-diisopropylethylamine at a volume ratio of 1:5), reacted in a dark room at 60°C for 6h, and cooled to At room temperature, add a large amount of water, then add ethyl acetate to extract, take the ...
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