A method for sweating and preparing wax for plastic processing
A technology of plastic and wax layer, which is applied in petroleum wax recovery, petroleum wax refining, etc., and can solve the problems of low production cycle and inability to produce wax products, etc.
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Embodiment 1
[0050] This embodiment includes: A: emulsification and B: sweating.
[0051] A: emulsification
[0052] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0053] (A1) Preparation of oil phase materials: Polyethylene wax (dropping melting point 85.8 °C; penetration (25 °C) 52 (10-1 mm); Penetration (55°C) > 200 (10 -1 mm). From the penetration at 25°C and 55°C, it can be seen that the raw material contains a large amount of low-melting point substances) 81.0Kg, after heating to 90°C and melting, add 1.2Kg of diethylene glycol fatty acid ester, 0.8Kg of polyoxypropylene stearic acid Ester, 0.3Kg sorbitan monopalmitate and 1.7Kg of tridecanoic acid, stir evenly.
[0054] (A2) Preparation of aqueous phase materials: prepare K with a concentration of 3.6% 2 CO 3 Solution, take 15.0Kg and heat to 95°C.
[0055] (A3) Emulsion preparation: Stir the oil phase material prepared in (A1) at a speed ...
Embodiment 2
[0070] This embodiment includes: A: emulsification and B: sweating.
[0071] A: emulsification
[0072] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0073] (A1) Preparation of oil phase material: Take 69.0Kg of polyethylene wax (same as Example 1) produced by the polyethylene plant of PetroChina Liaoyang Petrochemical Ethylene Plant, heat to 92°C and melt, add 2.3Kg of sorbitan monostearate Ester, 0.8Kg tetraethylene glycol monostearate, 0.4Kg lauryl betaine and 3.2Kg of pentadecanoic acid, stir well.
[0074] (A2) Preparation of aqueous phase materials: prepare Na with a concentration of 2.9% 2 CO 3 Solution, take 24.3Kg and heat to 96°C.
[0075] (A3) Emulsion preparation: Stir the oil phase material prepared in (A1) process at a speed of 750 rpm, add the water phase material prepared in (A2) process to the oil phase material, and continue stirring for 15 minutes to form an oil-in-...
Embodiment 3
[0080] This embodiment includes: A: emulsification and B: sweating.
[0081] A: emulsification
[0082] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0083] (A1) Preparation of oil phase materials: Take 78.0Kg of polyethylene wax (same as Example 1) produced by the polyethylene plant of PetroChina Liaoyang Petrochemical Ethylene Plant, heat to 93°C and melt, add 2.0Kg of diethylene glycol fatty acid ester, 0.6Kg sorbitan monopalmitate, 0.2Kg sodium alkylbenzene sulfonate and 2.2Kg palmitoleic acid, stir well.
[0084] (A2) Preparation of aqueous phase materials: prepare K with a concentration of 4.3% 2 CO 3 Solution, take 17.0Kg and heat to 97°C.
[0085] (A3) Emulsion preparation: Stir the oil phase material prepared in (A1) process at a speed of 500 rpm, add the water phase material prepared in (A2) process to the oil phase material, and continue stirring for 20 minutes to form an o...
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Abstract
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