Unlock instant, AI-driven research and patent intelligence for your innovation.

A method for sweating and preparing wax for plastic processing

A technology of plastic and wax layer, which is applied in petroleum wax recovery, petroleum wax refining, etc., and can solve the problems of low production cycle and inability to produce wax products, etc.

Active Publication Date: 2019-06-11
CHINA PETROLEUM & CHEM CORP +1
View PDF12 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0014] Compared with solvent separation, the sweating process is an intermittent operation, and the product yield is lower and the production cycle is longer, but the sweating process has the advantages of less investment, simple production process, low operating cost, safe production process, energy saving and no pollution to the environment, etc. Advantages, some manufacturers are still using this method to produce soap wax products
[0015] Over the years, the sweating method has been developed in terms of equipment and technology, such as CN89214332 (vertical square multi-section partition sweating tank), CN94223980.6 (dish-type sweating device), CN98233254.8 (paraffin wax sweating tank), CN200920033500.X (New paraffin sweating tank), CN201210508905.0 (a high-efficiency paraffin sweating device), CN201320127680.4 (tubular paraffin deoiling device), etc., have made improvements in sweating equipment; CN91206202 (a high-efficiency paraffin sweating tank) Improvements have been made in the sweating process, but these improvements still cannot produce wax products with a melting point above 70°C

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] This embodiment includes: A: emulsification and B: sweating.

[0051] A: emulsification

[0052] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.

[0053] (A1) Preparation of oil phase materials: Polyethylene wax (dropping melting point 85.8 °C; penetration (25 °C) 52 (10-1 mm); Penetration (55°C) > 200 (10 -1 mm). From the penetration at 25°C and 55°C, it can be seen that the raw material contains a large amount of low-melting point substances) 81.0Kg, after heating to 90°C and melting, add 1.2Kg of diethylene glycol fatty acid ester, 0.8Kg of polyoxypropylene stearic acid Ester, 0.3Kg sorbitan monopalmitate and 1.7Kg of tridecanoic acid, stir evenly.

[0054] (A2) Preparation of aqueous phase materials: prepare K with a concentration of 3.6% 2 CO 3 Solution, take 15.0Kg and heat to 95°C.

[0055] (A3) Emulsion preparation: Stir the oil phase material prepared in (A1) at a speed ...

Embodiment 2

[0070] This embodiment includes: A: emulsification and B: sweating.

[0071] A: emulsification

[0072] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.

[0073] (A1) Preparation of oil phase material: Take 69.0Kg of polyethylene wax (same as Example 1) produced by the polyethylene plant of PetroChina Liaoyang Petrochemical Ethylene Plant, heat to 92°C and melt, add 2.3Kg of sorbitan monostearate Ester, 0.8Kg tetraethylene glycol monostearate, 0.4Kg lauryl betaine and 3.2Kg of pentadecanoic acid, stir well.

[0074] (A2) Preparation of aqueous phase materials: prepare Na with a concentration of 2.9% 2 CO 3 Solution, take 24.3Kg and heat to 96°C.

[0075] (A3) Emulsion preparation: Stir the oil phase material prepared in (A1) process at a speed of 750 rpm, add the water phase material prepared in (A2) process to the oil phase material, and continue stirring for 15 minutes to form an oil-in-...

Embodiment 3

[0080] This embodiment includes: A: emulsification and B: sweating.

[0081] A: emulsification

[0082] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.

[0083] (A1) Preparation of oil phase materials: Take 78.0Kg of polyethylene wax (same as Example 1) produced by the polyethylene plant of PetroChina Liaoyang Petrochemical Ethylene Plant, heat to 93°C and melt, add 2.0Kg of diethylene glycol fatty acid ester, 0.6Kg sorbitan monopalmitate, 0.2Kg sodium alkylbenzene sulfonate and 2.2Kg palmitoleic acid, stir well.

[0084] (A2) Preparation of aqueous phase materials: prepare K with a concentration of 4.3% 2 CO 3 Solution, take 17.0Kg and heat to 97°C.

[0085] (A3) Emulsion preparation: Stir the oil phase material prepared in (A1) process at a speed of 500 rpm, add the water phase material prepared in (A2) process to the oil phase material, and continue stirring for 20 minutes to form an o...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
drop melting pointaaaaaaaaaa
boiling pointaaaaaaaaaa
drop melting pointaaaaaaaaaa
Login to View More

Abstract

The invention discloses a method for sweating and preparing wax for plastic processing. The method comprises the following steps: by taking a by-product, namely polyethylene wax, of polyethylene as a sweating raw material, emulsifying and sweating, thereby obtaining the target product. According to the method disclosed by the invention, an oil-soluble emulsifier and oil-soluble acid are dissolved in the sweating raw material to serve as an oil phase material on the basis of an ordinary sweating process, an inorganic salt solution serves as an aqueous phase material and is sweated after emulsification, and a tiny space is formed after bubbles and salt solution produced by reaction between the oil-soluble acid and the inorganic salt are discharged, so that the rapid discharge of the liquid components is facilitated. Meanwhile, the solid components and the liquid components can be forcibly separated by enabling airflow to carry out the liquid oil through a wax layer in the sweating process, so that low molecular weight components in the raw material can be effectively removed. The method disclosed by the invention has the advantages of low equipment investment, simple production process, low operating cost, safety, no solvent pollution and the like, and the prepared product can serve as an assistant for plastic processing.

Description

technical field [0001] The invention belongs to the technical field of special wax production, in particular to a method for sweating and preparing wax for plastic processing. Background technique [0002] Wax substances are commonly used additives in plastic processing, such as lubricants for various plastic processing. [0003] Lubricants used in plastic processing are to improve the fluidity and release properties of plastics, especially thermoplastics, during processing and molding. Molecules rub against each other, thereby improving the processing performance of plastics and improving the performance of products. At the same time, the lubricant can also act as a melting accelerator, anti-adhesion and antistatic agent, and slip agent. [0004] According to the mechanism of action of lubricants in plastic processing and molding, lubricants are divided into internal lubricants and external lubricants. Lubricants are widely used, rigid PVC, polyolefin, PS, ABS, phenolic ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10G73/36C10G73/42C08L101/00C08L91/06
CPCC08L91/06C08L101/00C10G73/36C10G73/42
Inventor 孙剑锋全辉李景斌王立言张志银张造根
Owner CHINA PETROLEUM & CHEM CORP