Preparation method of nano emulsion with embedded peppermint essential oil and application thereof in mouth wash

A technology of peppermint essential oil and nano-emulsion, which is applied to oral care, pharmaceutical formulations, cosmetic preparations and other directions, can solve the problems of single function of mouthwash, poor health care effect, etc., and achieves high market promotion value, few types of materials and processes simple effect

Inactive Publication Date: 2018-02-23
SHANGHAI INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Aiming at the above-mentioned technical problems in the prior art, the invention provides a kind of preparation method of nanoemulsion of entrapped peppermint essential oil and its application in

Method used

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  • Preparation method of nano emulsion with embedded peppermint essential oil and application thereof in mouth wash
  • Preparation method of nano emulsion with embedded peppermint essential oil and application thereof in mouth wash
  • Preparation method of nano emulsion with embedded peppermint essential oil and application thereof in mouth wash

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] 1. A mouthwash containing octenyl succinic acid short-chain glucan nanoparticles ternary system embedding peppermint essential oil nanoemulsion, the parts by weight of each component are as follows:

[0019]

[0020]

[0021] The preparation method of the mouthwash is as follows: according to the above proportion by weight, the ingredients are uniformly mixed, then added into ethanol, stirred and mixed evenly, and finally distilled water is added, stirred and mixed into a clear liquid, and the mouthwash is obtained.

[0022] 2. the preparation method of above-mentioned a kind of octenyl succinic acid short-chain glucan nanoparticle ternary system embedding peppermint essential oil nanoemulsion, comprises the following steps:

[0023] 1) Preparation of short-chain glucan: dissolve 10 g of waxy starch in water, heat gelatinization in an oil bath at 120° C., cool to 60° C., add pullulanase for debranching, and the addition of pullulanase The amount is 30 ASPU / g starc...

Embodiment 2

[0028] 1. A mouthwash containing octenyl succinic acid short-chain glucan nanoparticles ternary system embedding peppermint essential oil nanoemulsion, the parts by weight of each component are as follows:

[0029]

[0030] The preparation method of the mouthwash is as follows: according to the above proportion by weight, the ingredients are uniformly mixed, then added into ethanol, stirred and mixed evenly, and finally distilled water is added, stirred and mixed into a clear liquid, and the mouthwash is obtained.

[0031] 2. the preparation method of above-mentioned a kind of octenyl succinic acid short-chain glucan nanoparticle ternary system embedding peppermint essential oil nanoemulsion, comprises the following steps:

[0032] 1) Preparation of short-chain glucan: dissolve 10 g of waxy starch in water, heat gelatinization in an oil bath at 120° C., cool to 60° C., add pullulanase for debranching, and the addition of pullulanase The amount is 35 ASPU / g starch dry basis....

Embodiment 3

[0037] 1. a kind of mouthwash containing octenyl succinic acid short-chain glucan nanoparticle ternary system embedding mint essential oil nanoemulsion, is characterized in that:

[0038] The parts by weight of each composition are as follows:

[0039]

[0040] The preparation method of the mouthwash is as follows: according to the above proportion by weight, the ingredients are uniformly mixed, then added into ethanol, stirred and mixed evenly, and finally distilled water is added, stirred and mixed into a clear liquid, and the mouthwash is obtained.

[0041] 2. the preparation method of above-mentioned a kind of octenyl succinic acid short-chain glucan nanoparticle ternary system embedding peppermint essential oil nanoemulsion, comprises the following steps:

[0042] 1) Preparation of short-chain dextran: dissolve 15 g of waxy starch in water, heat gelatinization in an oil bath at 120° C., cool to 60° C., add pullulanase for debranching, and the addition of pullulanase T...

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Abstract

The invention provides a preparation method of a nano emulsion with embedded peppermint essential oil. The preparation method comprises a step of preparing short-chain glucan; a step of preparing octenyl succinic short-chain glucan; a step of preparing octenyl succinic short-chain glucan nano particles; and a step of preparing the nano emulsion with embedded peppermint essential oil. An octenyl succinic short-chain glucan solution is prepared first; then a peppermint essential oil solution is prepared and added to the corresponding octenyl succinic short-chain glucan solution to obtain an octenyl succinic short-chain glucan-peppermint essential oil nano emulsion. The invention also provides a mouth wash including following ingredients in parts by weight: 5-10 parts of calcium benzoate, 10-20 parts of aspartame, 10-15 parts of sorbitol, 10-15 parts of ethanol, 5-10 parts of sodium dodecyl sulfate, 50-70 parts of purified water and 1-5 parts of nano emulsion. With the help of the nano emulsion with embedded peppermint essential oil, long-term slow release of the peppermint essential oil can be achieved efficiently.

Description

technical field [0001] The invention belongs to the field necessary for human life, and relates to an oral care product, in particular to a preparation method of nanoemulsion embedding mint essential oil and its application in mouthwash. Background technique [0002] With the improvement of living standards, people also pay more and more attention to the quality of life. The traditional mouthwash has a single function, which can no longer meet the needs of people's pursuit of a healthy life. In recent years, due to the increasing awareness of consumer health care, more requirements have been put forward for mouthwash. In addition to cleaning teeth, some functions have been added to assist in the prevention of oral diseases and have a nursing and health care effect on the oral cavity. Mouthwash is a new product in the era of science and technology. It combines a variety of medicinal ingredients for the treatment of oral and throat diseases. caused by bad breath. [0003] Sh...

Claims

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Application Information

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IPC IPC(8): A61K8/92A61K8/73A61K8/55A61K8/06A61Q11/00
Inventor 冯涛王慧庄海宁赵宇曾小兰王晶晶吴阳张三丰夏艺玮李雪水梦竹陈忠秋王文欣王旭增童彦尊
Owner SHANGHAI INST OF TECH
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