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Surface modified nano metal oxide anti-wear self-repairing material and preparation method thereof

A self-healing material and nano-metal technology, which is applied in the field of polymer materials, can solve problems such as corrosion of mechanical equipment, and achieve the effects of protecting cold wear, stabilizing the structure, and reducing wear

Inactive Publication Date: 2018-07-20
烟台华恒节能科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, such extreme pressure antiwear agents are generally substances containing sulfur and phosphorus, wh

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0038] Example 1

[0039] A preparation method of surface-modified nano-alumina anti-wear and self-healing material, the steps are as follows:

[0040] (1) Surface modification of nano alumina

[0041] a. Soak 10g of nano alumina with a particle size of 50-100nm in 100g of aminosilane coupling agent KH182, and soak for 12h under inert gas protection at 20-25℃;

[0042] b. Transfer the nano-alumina soaked in step a to a three-necked flask, add 100g isotactic oligomeric polyvinyl alcohol and 120g sodium isooctyl succinate, heat in a water bath at 50°C, stir and disperse at 5000r / min for 2h;

[0043] c. Pump the mixture of step b into the ultrasonic oscillator, add 60g succinimide T161, adjust the ultrasonic dispersion power to 800W, the frequency to 24Hz, ultrasonic dispersion for 1h, filter, and wash with absolute ethanol at 80℃ Dry for 6 hours under the conditions to obtain surface-modified nano alumina;

[0044] (2) Add 10g of lanthanum borate, 4g of molybdenum dodecyl dithiophosphate ...

Example Embodiment

[0050] Example 2

[0051] A preparation method of surface-modified nano-alumina anti-wear and self-healing material, the steps are as follows:

[0052] (1) Surface modification of nano copper oxide

[0053] a. Soak 15g of nano-copper oxide with a particle size of 50-100nm in 100g of hydroxy-terminated silane coupling agent, and soak for 12h under inert gas protection at 20-25℃;

[0054] b. Transfer the nano-copper oxide soaked in step a to a three-necked flask, add 100g isotactic oligomeric polyvinyl alcohol and 120g sodium isooctyl succinate, heat in a water bath at 50°C, stir and disperse at 5000r / min for 2h;

[0055] c. Pump the mixture of step b into an ultrasonic oscillator, add 50g of succinimide T161, adjust the ultrasonic dispersion power to 1200W, frequency to 24Hz, ultrasonic dispersion for 1h, filter, and wash with absolute ethanol at 80℃ Dry for 6 hours under the conditions to obtain surface-modified nano alumina;

[0056] (2) Add 10g of lanthanum borate, 4g of molybdenum do...

Example Embodiment

[0062] Example 3

[0063] A preparation method of surface-modified nano-alumina anti-wear and self-healing material, the steps are as follows:

[0064] (1) Surface modification of nano chromium oxide

[0065] a. Soak 10g of nano chromium oxide with a particle size of 50-100nm in 100g of aminosilane coupling agent KH182, and soak for 11h under inert gas protection at 20-25℃;

[0066] b. Transfer the nano-chromium oxide soaked in step a to a three-necked flask, add 100g isotactic oligomeric polyvinyl alcohol and 120g sodium isooctyl succinate, heat in a water bath at 50°C, stir and disperse at 5000r / min for 2h;

[0067] c. Pump the mixture of step b into the ultrasonic oscillator, add 60g succinimide T161, adjust the ultrasonic dispersion power to 800W, the frequency to 24Hz, ultrasonic dispersion for 1h, filter, and wash with absolute ethanol at 80℃ Dry for 6 hours under the conditions to obtain surface-modified nano-chromium oxide;

[0068] (2) Add 10g of cerium borate, 4g of molybdenum...

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Abstract

The invention relates to a surface modified nano metal oxide anti-wear self-repairing material and a preparation method thereof. The prepared product is good in oil solubility, the generation of sediment of the product in lubricating oil, which affects the extreme pressure and anti-wear performance of the product, is avoided, and the product can be dissolved in lubricating oil of all models. The product has excellent load resistance and extreme pressure and anti-wear performance and is suitable for heavy-duty mechanical lubrication and extreme pressure anti-wear; and the product has a smart self-repairing function for scratches and wear of the surface of a friction part. When the surface modified nano metal oxide anti-wear self-repairing material is used for an engine, oil can be saved by15% or more, the engine noise is reduced by 15%, the material has functions of anti-wear and noise reduction and particularly can greatly reduce wear during cold start of an automobile and better protect the engine from cold wear; the oil change period is prolonged by one time or more (engine oil is replaced each time the automobile travels over 10000 to 15000 km), the catalytic oxidation of the lubricating oil through metal ions under high temperature is prevented, and the service life of the lubricating oil is prolonged.

Description

technical field [0001] The invention relates to an anti-wear self-repair material, in particular to a surface-modified nanometer metal oxide anti-wear self-repair material and a preparation method thereof, belonging to the field of polymer materials. Background technique [0002] Lubricating oil is called the blood of industry. Lubricating technology is the most effective anti-wear and anti-friction measure for mechanical systems. Improving the performance of lubricating oil and developing environmentally friendly new lubricating additives are inevitable to solve the increasing consumption of lubricating oil industry and protect the environment. need. In the 21st century, along with the development of modern industrial technology, industrial machinery and equipment continue to develop in the direction of high power, miniaturization, automation, high precision, increased power, improved efficiency, and increased reliability. Larger loads, higher temperatures and harsher envi...

Claims

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Application Information

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IPC IPC(8): C10M125/10C10M177/00C10M169/04C10N30/06
CPCC10M125/10C10M169/048C10M177/00C10M2201/062C10M2201/087C10M2201/14C10M2203/1025C10M2205/0285C10M2205/16C10M2209/04C10M2215/086C10M2219/044C10M2223/045C10N2030/06C10N2030/54C10N2030/72C10N2030/76C10N2010/12C10N2020/02C10N2010/06C10N2010/02C10N2020/06C10N2010/04
Inventor 任朋成
Owner 烟台华恒节能科技有限公司
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