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A preparation method of inerting powder for rapidly suppressing deflagration of wood flour

A technology of inerting powder and wood powder, which is applied in graphite, fire rescue, etc., can solve the problems of inerting and suppressing explosion of inorganic silicon powder, difficulty in uniform mixing of combustible dust, and less research on inerting and suppressing explosion. Achieve the effects of broadening resource utilization and high value-added utilization, mild preparation conditions, and rapid combustion suppression of wood powder

Active Publication Date: 2021-07-06
XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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Problems solved by technology

Common organic dusts such as starch, wood flour, and flour all have potential explosion hazards. However, the current research on dust explosions mainly focuses on the inerting treatment and explosion suppression technology for dense dust such as coal powder, aluminum powder, magnesium powder, and titanium powder. And the inerting agent used is mainly ammonium dihydrogen phosphate, aluminum hydroxide, calcium carbonate, ammonium bicarbonate, etc. and their compound, because it is difficult to mix evenly with combustible dust, resulting in a low explosion suppression effect
In addition, in the industry and trade, especially in the production and processing of wooden building materials, flammable and explosive light wood powders are easy to be produced, and there are few researches on inerting and explosion suppression of them, and no use of inorganic siliceous powders has been seen. Research Report on Inerting Explosion Suppression

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  • A preparation method of inerting powder for rapidly suppressing deflagration of wood flour

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Embodiment 1

[0019] This example provides a method for preparing an inert powder that quickly suppresses the deflagration of wood flour. The NaOH of the formula is dissolved in quantitative water, and the concentration of the NaOH substance is 8mol*L -1 , and place it in a constant temperature water bath at 60° C. to obtain a chemical modifier solution.

[0020] Then slowly add 20g of expandable graphite into 100mL of NaOH solution in a magnetic stirrer, stir for 15min, then ultrasonicate for 5min and impregnate in air isolation, and finally wash with water until pH = 7, filter, dry, and grind to obtain an inert powder , and fully mix it with wood powder in a mortar (inerting powder: wood powder = 1:10, wt%), and use 1.2L Ha Terman tube tests its explosion, explosion pressure rise rate, maximum explosion pressure, etc. In order to further confirm its combustion characteristics, its heat release performance was tested with a cone calorimeter (about 550°C) with reference to GB / T 16172-2007 ...

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Abstract

The present invention proposes a method for preparing an inerted powder for quickly inhibiting the deflagration of wood powder. Chemically modified expandable graphite is used as the inerting powder for inhibiting the deflagration of wood powder. , NaOH solution chemical modifier, respectively through the process of dissolving, stirring, ultrasonic, dipping, washing, filtration, drying and other processes to prepare inert powder that can inhibit the deflagration of wood powder. The innovation of the invention lies in that the NaOH modified expandable graphite is used as the inerting agent for the first time to remove organic combustible impurities, strengthen its characteristics such as suffocation and flame retardant, and prepare the graphite-based flame-suppressing and inerting agent, which has the advantages of low cost, rapid flame retardant, The characteristics of simple process and strong inerting performance have opened up the research of expandable graphite in the design of combustible dust inerting.

Description

technical field [0001] The invention belongs to the technical field of chemical building materials and fire safety, and in particular relates to a preparation method of an inerting powder for rapidly suppressing deflagration of wood powder. Background technique [0002] Dust explosions in the industrial manufacturing process have caused catastrophic property losses and personal injuries to human society. Since a large amount of combustible dust is easily produced in the industrial manufacturing process, for organic dust with low minimum ignition energy, when its concentration reaches above the lower explosion limit When the explosion occurs, tiny sparks can easily cause an explosion, especially in a confined space, a secondary explosion is more likely to occur, resulting in serious economic losses and social problems. Therefore, inerting and suppressing combustible dust explosion hazards has become an important safety prevention and control measure and development trend in t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B32/21A62C3/04
CPCA62C3/04C01B32/21
Inventor 王亚超赵江平崔晓红李华韩煜久杨宏刚张田娇周钦君李雨星王若琪
Owner XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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