A preparation method of inert powder for suppressing starch deflagration

A technology of inerting powder and deflagration, which is applied in the fields of silicon oxide, silicon dioxide, fire rescue, etc. It can solve the problems of low explosion suppression effect, no inorganic silicon powder inerting explosion suppression, and difficulty in uniform mixing of combustible dust, etc. , to achieve the effects of excellent explosion suppression performance, widening resource utilization and high value-added utilization, and mild preparation conditions

Active Publication Date: 2021-07-20
XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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Problems solved by technology

Common organic dusts such as starch, wood flour, and flour all have potential explosion hazards. However, the current research on dust explosions mainly focuses on the inerting treatment and explosion suppression technology for dense dust such as coal powder, aluminum powder, magnesium powder, and titanium powder. And the inerting agent used is mainly ammonium dihydrogen phosphate, aluminum hydroxide, calcium carbonate, ammonium bicarbonate, etc. and their compound, because it is difficult to mix uniformly with combustible dust, resulting in a low explosion suppression effect; in addition, in In the industry and trade industry, especially food production and processing enterprises, it is easy to produce flammable and explosive light organic dust, such as starch, flour, etc., and there are few studies on its inertization and explosion suppression, and no inorganic silicon powder is used. Research Report on Inerting Explosion Suppression

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  • A preparation method of inert powder for suppressing starch deflagration
  • A preparation method of inert powder for suppressing starch deflagration
  • A preparation method of inert powder for suppressing starch deflagration

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Embodiment 1

[0024] This example provides a preparation method of an inert powder that suppresses starch deflagration. NaOH is dissolved in quantitative water, and the concentration of NaOH is 8mol*L -1 , and place it in a constant temperature water bath at 60° C. to obtain a chemical modifier solution.

[0025] Then slowly add 100g of diatomaceous earth into 200mL of NaOH solution in a magnetic stirrer, stir for 15min, then ultrasonicate for 5min and impregnate in air isolation, and finally wash with water until pH = 7, filter, dry, and grind to obtain an inert powder , fully mix it with starch in a mortar (inert powder: starch = 1:10, wt%), and use 1.2L Hartmann Tube test its explosion, explosion pressure rise rate, maximum explosion pressure, etc. In order to further confirm its combustion characteristics, its heat release performance was tested with a cone calorimeter (about 550°C) with reference to the GB / T 16172-2007 "Test Method for Heat Release Rate of Building Materials". The res...

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Abstract

The present invention proposes a method for preparing an inert powder for inhibiting starch deflagration, using chemically modified diatomite as the following inert powder for inhibiting starch deflagration, and the preparation process is as follows: first-grade diatomite for building materials is used as The raw material uses NaOH solution as a chemical modifier, and the inert powder that can inhibit starch deflagration is prepared through processes such as dissolution, stirring, ultrasonication, impregnation, water washing, filtration, drying, and grinding. The innovation of this invention is that NaOH modified diatomaceous earth is used as inert agent for the first time to remove organic combustible impurities, strengthen its characteristics such as large specific surface area, high porosity and adsorption rate, low thermal conductivity and low density, and prepare inorganic silicic acid Salt flame-inhibiting inerting agent, which has the characteristics of low cost, simple process, and strong inerting performance, has opened up the research of inorganic silicon powder in the inerting design of combustible dust.

Description

technical field [0001] The invention belongs to the technical field of chemical building materials and fire safety, and in particular relates to a method for preparing an inert powder capable of suppressing starch deflagration. Background technique [0002] Dust explosions in the industrial manufacturing process have caused catastrophic property losses and personal injuries to human society. Since a large amount of combustible dust is easily produced in the industrial manufacturing process, for organic dust with low minimum ignition energy, when its concentration reaches above the lower explosion limit When the explosion occurs, tiny sparks can easily cause an explosion, especially in a confined space, a secondary explosion is more likely to occur, resulting in serious economic losses and social problems. Therefore, inerting and suppressing combustible dust explosion hazards has become an important safety prevention and control measure and development trend in the industry a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B33/12A62C3/04
CPCA62C3/04C01B33/12
Inventor 王亚超赵江平崔晓红李华韩煜久杨宏刚张田娇周钦君李雨星王若琪
Owner XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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