Application of a kind of mesoporous carbon sphere in making saturable absorber
A saturable absorption, mesoporous carbon technology, used in laser parts, electrical components, phonon exciters, etc.
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Embodiment 1
[0030] Example 1: A saturable absorber prepared by mixing mesoporous carbon spheres and a film-forming agent—sodium carboxymethylcellulose (NaCMC) and used for mode-locked laser output at 1 μm;
[0031] 1. Sample preparation process
[0032]The mesoporous carbon spheres are synthesized by the "silica template method", that is, soluble phenolic resin is used as a precursor, tetraethyl orthosilicate (TEOS) is used as a precursor, and hexadecyl trimethyl chloride Amine (CTAC) is the template; first, mix 10mL (25wt%) ammonia water, 4-8mL ethanol aqueous solution, 1.04g (25wt%) CTAC solution and 19mL deionized water in a beaker, and keep stirring for 30 minutes , then add 0.2g of resorcinol to the solution, continue stirring for 30 minutes, inject 0.72mL of TEOS and 0.28mL of formaldehyde solution into the above solution, and continue stirring at 30°C for 24 hours; The solid product was obtained by machine, and dried naturally at 80°C; the dried solid product was fed with nitrogen...
Embodiment 2
[0037] Example 2: A saturable absorber prepared by mixing mesoporous carbon spheres and a film-forming agent—sodium carboxymethylcellulose (NaCMC) and used for Q-switched laser output at 1.56 μm band;
[0038] 1. Sample preparation process
[0039] The mesoporous carbon spheres are synthesized by the "silica template method", that is, soluble phenolic resin is used as a precursor, tetraethyl orthosilicate (TEOS) is used as a precursor, and hexadecyl trimethyl chloride Amine (CTAC) is the template; first, mix 10mL (25wt%) ammonia water, 4-8mL ethanol aqueous solution, 1.04g (25wt%) CTAC solution and 19mL deionized water in a beaker, and keep stirring for 30 minutes , then add 0.2g of resorcinol to the solution, continue stirring for 30 minutes, inject 0.72mL of TEOS and 0.28mL of formaldehyde solution into the above solution, and continue stirring at 30°C for 24 hours; The solid product was obtained by machine, and dried naturally at 80°C; the dried solid product was fed with ...
Embodiment 3
[0044] Example 3: A saturable absorber mixed with mesoporous carbon spheres and a film-forming agent—sodium carboxymethylcellulose (NaCMC) and used for Q-switched laser output at 2 μm band;
[0045] 1. Sample preparation process
[0046] The mesoporous carbon spheres are synthesized by the "silica template method", that is, soluble phenolic resin is used as a precursor, tetraethyl orthosilicate (TEOS) is used as a precursor, and hexadecyl trimethyl chloride Amine (CTAC) is the template; first, mix 10mL (25wt%) ammonia water, 4-8mL ethanol aqueous solution, 1.04g (25wt%) CTAC solution and 19mL deionized water in a beaker, and keep stirring for 30 minutes , then add 0.2g of resorcinol to the solution, continue stirring for 30 minutes, inject 0.72mL of TEOS and 0.28mL of formaldehyde solution into the above solution, and continue stirring at 30°C for 24 hours; The solid product was obtained by machine, and dried naturally at 80°C; the dried solid product was fed with nitrogen in...
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