Dispersible solid preparation for preventing fruit drop and its preparation method and use

A technology of dispersant and fruit, which is applied in the field of dispersible solid preparations and its preparation, can solve the problems of 1-methylcyclopropene effect reduction, unrecorded preparation, uneven drug distribution, etc., achieve good thermal storage stability, prevent The effect of mutual aggregation and simple processing technology

Active Publication Date: 2019-09-13
CHINA AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If directly process citrus with 1-methylcyclopropene, because the type of preparation directly used by 1-methylcyclopropene is a fumigant, the effect of the fumigant as spraying is very unsatisfactory; if it is made into a preparation, but the patent document There is no record of what type of preparation was made, let alone what advantages or technical problems it overcomes when making this type of preparation for spraying citrus
[0006] In short, on the one hand, for 1-methylcyclopropene fumigant, the 1-methylcyclopropene fumigant is put into water, the active ingredient 1-methylcyclopropene is released in a closed environment, and the target crops are treated in a closed environment. , and when it is used as spraying, it is impossible to seal the field orchard, which will greatly reduce the effect of 1-methylcyclopropene and greatly reduce the economic value; on the other hand, 1-methylcyclopropene fumigant has no special excipient The agent cannot be applied with oil or water, and excellent suspension performance and dispersion performance cannot be obtained, resulting in uneven distribution of the agent, clogging of the nozzle, etc.

Method used

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  • Dispersible solid preparation for preventing fruit drop and its preparation method and use
  • Dispersible solid preparation for preventing fruit drop and its preparation method and use
  • Dispersible solid preparation for preventing fruit drop and its preparation method and use

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] Embodiment 1: 0.033% 1-methylcyclopropene microcapsule wettable powder

[0042] The selection and ratio of original drug and additives are: 1-methylcyclopropene microcapsule granule 1%, dispersant polycarboxylate 5%, wetting agent saponin powder 3%, stabilizer 2,6-ditert-tert Butyl-4-methylphenol 1%, solid carrier calcined kaolin 90%.

[0043] Preparation methods include:

[0044] 1) Pulverization: 1% of 1-methylcyclopropene microcapsules, 5% of dispersant polycarboxylate, 3% of wetting agent saponin powder, 1% of stabilizer 2,6-ditertiary Butyl-4-methylphenol is mixed with 90% solid carrier calcined kaolin, mechanically pulverized, airflow pulverized, and then mixed;

[0045] 2) Detection: After the determination of the control indicators, the water in the final product is 2.33%, the pH value is 6.37, the mass suspension rate is 98.12%, the wetting time is 43.0s, and the fineness (wet sieve, passing through a 45μm test sieve) is 99.2 %, the content of 1-methylcyclop...

Embodiment 2

[0046] Embodiment 2: 0.825% 1-methylcyclopropene microcapsule wettable powder

[0047] The selection and ratio of the original drug and additives are: 1-methylcyclopropene microcapsule granule 25%, dispersant naphthalenesulfonate formaldehyde condensate 5%, wetting agent sodium lauryl sulfate 3%, stabilizer Tert-butyl p-hydroxyanisole 1%, solid carrier kaolin 66%.

[0048] Preparation methods include:

[0049] 1) Pulverization: 25% of 1-methylcyclopropene microcapsules, 5% of dispersant naphthalenesulfonate formaldehyde condensate, 3% of wetting agent sodium lauryl sulfate, 1% of stabilizer tert-butyl-p-hydroxyanisole is mixed with 66% solid carrier kaolin, mechanically pulverized, then air-jet pulverized, and then mixed;

[0050] 2) Detection: After the determination of the control indicators, the water in the final product is 3.13%, the pH value is 6.78, the mass suspension rate is 97.23%, the wetting time is 35.0s, and the fineness (wet sieve, passing through a 45μm test ...

Embodiment 3

[0051] Embodiment 3: 1.650% 1-methylcyclopropene microcapsule wettable powder

[0052] The selection and ratio of the original drug and additives are: 1-methylcyclopropene microcapsules 50%, dispersant sodium lignosulfonate 5%, wetting agent pull-off powder 3%, stabilizer propyl gallate 1 %, solid carrier bentonite 41%.

[0053] Preparation methods include:

[0054] 1) Pulverization: 50% 1-methylcyclopropene microcapsules, 5% dispersant sodium lignosulfonate, 3% wetting agent pull apart powder, 1% stabilizer propyl gallate and 41% of the solid carrier bentonite is mixed, mechanically pulverized, then jet pulverized, and then mixed;

[0055] 2) Detection: After the determination of the control indicators, the water in the final product is 2.69%, the pH value is 7.43, the mass suspension rate is 98.56%, the wetting time is 22.0s, and the fineness (wet sieve, passing through a 45μm test sieve) is 99.6 %, 1-methylcyclopropene content is 1.648%, the product is qualified, and 1.6...

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Abstract

The invention discloses a dispersible solid preparation for preventing fruits from falling, and a preparation method and application thereof. The dispersible solid preparation is prepared from the following mass percentages of components: 1%-95% of 1-methylcyclopropene microcapsules, 1%-10% of dispersant, 1%-10% of wetting agent, 0.1%-10% of stabilizer, and the balance of solid carrier, wherein the content of 1-methylcyclopropene in the dispersible solid preparation is 0.01%-4.75%. The dispersible solid preparation obtained by the invention has low moisture content, almost neutral pH value, excellent suspension property, wettability and heat storage stability, and the fineness up to 99.6%, so the preparation will not block nozzles. The sedimentation speed of the preparation is low, so thepreparation can continue to play drug roles for a certain period after application, satisfy the requirement of uniform distribution of medicinal liquid in an open orchard environment system and guarantee the action time, and has a very good effect of preventing fruit falling during harvest, and can prolong harvest time.

Description

technical field [0001] The invention relates to a preparation for preventing fruit drop, in particular to a dispersible solid preparation for preventing fruit drop and its preparation method and application. Background technique [0002] In order to reduce the loss of the fruit industry, relevant work can be carried out from two aspects of preventing fruit drop and post-preservation. At present, the method of preventing fruit drop mainly starts from two aspects: one is the cultural method, which suppresses the balance between plant growth and reproductive growth through fertilizer and water control, thinning flower buds, flowering girdling, etc.; the other is the use of plant growth regulation to To regulate the physiological state of fruit trees, it is generally used in the current production to spray gibberellin on the orchard before and after flowering and spray NAA before harvest. However, although spraying gibberellin can prevent flower and fruit drop, it will make the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N27/00A01N25/14A01P21/00A01G7/06
Inventor 吴学民郭鑫宇张振华逄森赵锐
Owner CHINA AGRI UNIV
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