A pressure-responsive aromatic sustained-release microcapsule, its preparation method and its application
A fragrance slow-release and microcapsule technology, which is applied in the direction of microcapsule preparation, microsphere preparation, essential oil/fragrance, etc., can solve the problems of poor fragrance release effect, waste of raw materials, and low service life
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Embodiment 1
[0043] A method for preparing pressure-responsive aromatic slow-release microcapsules, the specific steps are as follows:
[0044] (1) Preparation of porous silica powder adsorbed with plant essential oil: use porous silica powder as the adsorption material to absorb plant essential oil at 80°C for 45min, filter while hot and wash with ethanol three times, and then Dry at room temperature and -0.05MPa for 48 hours to obtain porous silica powder adsorbed with essence, wherein the average particle size of the porous silica powder is 1.0 μm, the porosity is 30%, and the specific surface area is 300m 2 / g, the mass ratio of silicon dioxide powder and plant essential oil is 1:100;
[0045] (2) Disperse the porous silica powder adsorbed with plant essential oil in deionized water whose stirring speed is 6000r / min;
[0046] (3) After adding nano-silica, natural latex and cross-linking agent XR-500 and cross-linking at 60°C for 15 minutes, cross-linking at 85°C for 10 minutes to prep...
Embodiment 2
[0058] A method for preparing pressure-responsive aromatic slow-release microcapsules, the specific steps are as follows:
[0059] (1) Preparation of porous silica powder adsorbed with grapefruit essence: use porous silica powder as the adsorption material to absorb grapefruit essence at 60°C for 25 minutes, filter while hot and wash with ethanol three times, Then dry at room temperature and -0.05MPa for 48 hours to obtain a porous silica powder adsorbed with essence, wherein the average particle diameter of the porous silica powder is 0.5 μm, the porosity is 30%, and the specific surface area is 150m 2 / g, the mass ratio of silicon dioxide powder and grapefruit essence is 1:10;
[0060] (2) Disperse the porous silica powder adsorbed with grapefruit essence in deionized water whose stirring speed is 3000r / min;
[0061] (3) After adding nano-silica, natural latex and cross-linking agent XR-500, cross-linking at 45°C for 15 minutes, and then cross-linking at 70°C for 10 minutes...
Embodiment 3
[0071] A method for preparing pressure-responsive aromatic slow-release microcapsules, the specific steps are as follows:
[0072] (1) Preparation of porous silica powder adsorbed with lemon essence: use porous silica powder as the adsorption material, after adsorbing lemon essence at 75°C for 35 minutes, filter while hot and wash with ethanol three times, then in room temperature , Dry for 48 hours under the condition of -0.05MPa to obtain porous silica powder with essence adsorbed, wherein the average particle size of the porous silica powder is 0.5μm, the porosity is 30%, and the specific surface area is 200m 2 / g, the mass ratio of silicon dioxide powder and lemon essence is 1:50;
[0073] (2) Disperse the porous silica powder adsorbed with lemon essence in deionized water whose stirring speed is 6000r / min;
[0074] (3) After adding nano-silica, natural latex and cross-linking agent XR-500, cross-linking at 60°C for 15 minutes, cross-linking at 85°C for 5 minutes to prepa...
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