Resourceful treatment method of organic medical wastes
A technology of medical waste and treatment method, applied in the field of hazardous waste recycling, can solve the problem of high cost and achieve the effect of short route, simple operation and carbon emission reduction
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Embodiment 1
[0021] Weigh 101.25g of alkylated waste sulfuric acid (acid concentration is 90.3%, containing 6.8% of organic matter) in a round bottom flask (250mL), add organic medical waste of 30% of waste acid quality and ethylene tar of 5% of medical waste quality, Raise from room temperature to 160°C, then maintain for 3.5h, cool to room temperature, weigh 1 times the weight of waste acid and add it to a round bottom flask, stir for 30min, repeat washing with water and stir for 3 times to obtain the filtrate (dilute sulfuric acid Solution) and filter cake (carbon material), collect filtrate in the beaker, the COD value of test filtrate is 361.2mg L -1 , slowly add ammonia water (25-28wt%) under stirring conditions until the solution is neutral, then evaporate the solution until 51.24 g of ammonium sulfate crystals are precipitated. The filter cake was washed with deionized water until neutral, and dried at 110° C. and 0.1 MPa for 2 hours to obtain 38.62 g of carbon materials.
Embodiment 2
[0023] Weigh 146.4g of alkylated waste sulfuric acid (acid concentration is 89.2%, containing 6.8% of organic matter) in a round bottom flask (250 mL), add organic medical waste equal to the quality of waste acid and 1-1% of organic medical waste. Hexyne, raised from room temperature to 250°C, then maintained for 0.5h, cooled to room temperature, weighed water with 1 times the mass of waste acid, added to the round bottom flask, stirred for 30min, repeated washing with water and stirring 3 times to obtain the filtrate (dilute sulfuric acid solution) and filter cake (carbon material), collect the filtrate in the beaker, the COD value of the test filtrate is 528.7mg L -1 , Add ammonia water (25-28wt%) slowly under stirring conditions until the solution is neutral, then evaporate the solution until 48.6 g of crystals are precipitated. The filter cake was washed with deionized water until neutral, and dried at 150° C. and 0.05 MPa for 3 hours to obtain 138.62 g of carbon materials...
Embodiment 3
[0025] Take by weighing 71.6g of sulfuric acid in a round bottom flask (250mL), add 2 times of organic medical waste of acid quality and 10% 1,4-dioxane of organic medical waste quality, from room temperature to 200 ℃, then Maintain for 2 hours, cool to room temperature, weigh 1 times the mass of sulfuric acid and add it to a round bottom flask, stir for 30 minutes, repeat washing with water and stirring for 3 times to obtain filtrate (dilute sulfuric acid solution) and filter cake (carbon material), collect the filtrate into the beaker, the COD value of the test filtrate is 3428.3mg L -1, while stirring, slowly add ammonia water (25-28wt%) until the solution is neutral, and then evaporate the solution until 50.3 g of crystals are precipitated. The filter cake was washed with deionized water until neutral, and dried at 200° C. and 0.01 MPa for 3 hours to obtain 126.01 g of carbon materials.
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