Method for preparing flame retardant by utilizing modifying technology and compounding technology

A flame retardant and technology, which is applied in the field of preparing flame retardants by using modification technology and compounding technology to achieve the effects of improving various properties, prolonging the usable life, and reducing the consumption of antimony

Inactive Publication Date: 2019-01-18
广西华锑科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The invention provides a method for preparing a flame retardant using modification technology and comp

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0045] Example 1

[0046] A flame retardant, in parts by mass, including the following raw materials: 12 parts of polybutylene terephthalate, 60 parts of antimony trioxide, 20 parts of magnesium-aluminum layered double hydroxide, basic carbonic acid 0.5 part of salt, 1 part of organic ammonium bromide, 1.5 parts of methyl silicone oil, 1 part of acrylate, 4 parts of dispersant.

[0047] The melt mass flow rate of the polybutylene terephthalate is 30 g / 10 min.

[0048] The antimony trioxide is a full cubic crystal type, with an average particle size of 1.0-3 μm, a purity of 99.67-99.81%, and a whiteness of 95-98.

[0049] The basic carbonate is magnesium aluminum basic sodium carbonate.

[0050] The organic ammonium bromide is tetrabutylammonium bromide.

[0051] The dispersant is polyethylene wax.

[0052] The method for preparing a flame retardant using modification technology and compounding technology includes the following steps:

[0053] Step 1. Polybutylene terephthalate drying: usi...

Example Embodiment

[0058] Example 2

[0059] A flame retardant, in parts by mass, including the following raw materials: 12 parts of polybutylene terephthalate, 70 parts of antimony trioxide, 10 parts of magnesium aluminum layered double hydroxide, and basic carbonic acid 0.5 part of salt, 1 part of organic ammonium bromide, 1.5 parts of methyl silicone oil, 1 part of acrylate, 4 parts of dispersant.

[0060] The melt mass flow rate of the polybutylene terephthalate is 5-40 g / 10 min.

[0061] The antimony trioxide is a full cubic crystal type, with an average particle size of 2-5 μm, a purity of 99.71-99.85%, and a whiteness of 96-99.

[0062] The basic carbonate is magnesium aluminum basic potassium carbonate.

[0063] The organic ammonium bromide is cetyl ammonium bromide.

[0064] The dispersant is silicone masterbatch.

[0065] The method for preparing a flame retardant using modification technology and compounding technology includes the following steps:

[0066] Step 1. Polybutylene terephthalate dryi...

Example Embodiment

[0071] Example 3

[0072] A flame retardant, in parts by mass, including the following raw materials: 12 parts of polybutylene terephthalate, 60 parts of antimony trioxide, 20 parts of magnesium-aluminum layered double hydroxide, basic carbonic acid 1 part of salt, 0.5 part of organic ammonium bromide, 1 part of methyl silicone oil, 1.5 parts of acrylate, 4 parts of dispersant.

[0073] The melt mass flow rate of the polybutylene terephthalate is 10-42 g / 10 min.

[0074] The antimony trioxide is a full cubic crystal type, with an average particle size of 1.2-4 μm, a purity of 99.65-99.82%, and a whiteness of 95-99.

[0075] The basic carbonate is magnesium aluminum basic sodium carbonate.

[0076] The organic ammonium bromide is cetyl ammonium bromide.

[0077] The dispersant is polyethylene wax.

[0078] The method for preparing a flame retardant using modification technology and compounding technology includes the following steps:

[0079] Step 1. Polybutylene terephthalate drying: usin...

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Abstract

The invention discloses a method for preparing a flame retardant by utilizing a modifying technology and a compounding technology, and belongs to the technical field of flame retardant preparation. The flame retardant is prepared from the following raw materials: polybutylene terephthalate, antimonous oxide, magnalium layered double hydroxide, subcarbonate, organic ammonium bromide, methyl silicone oil, acrylic ester and a dispersant. The flame retardant is prepared by polybutylene terephthalate drying, surface modification of the antimonous oxide, surface modification of magnalium layered double hydroxide, mixing, granulating, screening, drying and the like. According to the method, the modifying and synergizing technical means is adopted, the addition amount of the flame retardant is 10-20 percent, the antimony part is substituted by comprehensive compounding; and in the development of the product in the invention, the consumption of antimony can be greatly reduced, and the utilization limit of the antimony resource can be prolonged.

Description

technical field [0001] The invention belongs to the technical field of preparation of flame retardants, and in particular relates to a method for preparing flame retardants using modification technology and compounding technology. Background technique [0002] The ideal goal of people using flame retardants is to use a small amount of flame retardants to achieve high-efficiency flame retardancy. The use process is simple, low cost and durable, with good stability, non-toxicity, and safety. In practical applications, a single-component flame retardant cannot meet all the above requirements, and compounding methods are required to integrate the performance advantages of various flame retardants to meet people's expected use requirements. Nowadays, people's awareness of environmental protection is gradually increasing. While paying attention to their own health, they actively respond to the government's call and pay attention to environmental protection. Since the 18th Nationa...

Claims

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Application Information

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IPC IPC(8): C08L67/02C08L83/04C08K9/04C08K9/06C08K3/22C08K7/00C08K3/26C08K13/06
CPCC08L67/02C08L2201/02C08L83/04C08K9/04C08K9/08C08K3/2279C08K7/00C08K3/26C08K13/06
Inventor 雷圆戴新王涛蓝莉荔潘善初
Owner 广西华锑科技有限公司
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