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Bio-pesticide containing rice dreg residual oil glycerin fatty acid ester and preparation method thereof

A technology for fatty acid glycerides and biological pesticides, which is applied in the field of biological pesticides containing fatty acid glycerides of rice residue residue oil and the field of preparation thereof, and achieves the effects of easy industrialization and large-scale production, wide insecticidal spectrum and good killing effect.

Active Publication Date: 2019-03-26
上海沪联生物药业(夏邑)股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is currently no relevant report on the combined use of fatty acid glycerides of rice dregs and Bacillus thuringiensis for the preparation of biopesticides

Method used

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  • Bio-pesticide containing rice dreg residual oil glycerin fatty acid ester and preparation method thereof
  • Bio-pesticide containing rice dreg residual oil glycerin fatty acid ester and preparation method thereof
  • Bio-pesticide containing rice dreg residual oil glycerin fatty acid ester and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] The preparation of embodiment 1 rice dregs residual oil fatty acid glyceride

[0034] S1: Mix the rice dregs and petroleum ether according to the ratio of solid to liquid 1g:7mL, extract for 3 hours at a temperature of 20°C and an oscillation rate of 120r / min, then suction filter, and place the obtained suction filtrate in a water bath Heat in the pot to remove the volatile solvent, and obtain the rice dregs residual oil extract;

[0035] S2: Add the rice dregs residual oil extract to the reaction kettle, and continue for 30 minutes at a temperature of 65°C and a vacuum of 0.12MPa to remove volatile impurities; wait until the temperature of the rice dregs residual oil extract drops to 50°C When adding 2% m / m of lipase RM IM and 10% m / m of glycerol, the vacuum is 0.10MPa, and the condition of feeding nitrogen is carried out to continue the reaction until the acid value of the rice dregs residual oil extract drops When it is below 4KOH / mg.g, the reaction is stopped, and ...

Embodiment 2

[0036] The preparation of embodiment 2 rice dregs residual oil fatty acid glyceride

[0037] S1: Mix rice dregs and petroleum ether according to the ratio of solid to liquid 1g:6mL, extract for 2 hours at a temperature of 25°C and an oscillation rate of 130r / min, then suction filter, and place the obtained suction filtrate in a water bath Heat in the pot to remove the volatile solvent, and obtain the rice dregs residual oil extract;

[0038] S2: Add the rice dregs residual oil extract to the reactor, and continue for 25 minutes at a temperature of 75°C and a vacuum of 0.09MPa to remove volatile impurities; wait until the temperature of the rice dregs residual oil extract drops to 60°C When adding 1% m / m of lipase and 5% m / m of glycerin, the vacuum is 0.08MPa, and the continuous reaction is carried out under the condition of feeding nitrogen, until the acid value of the rice dregs residual oil extract is reduced to 4KOH When the lipase RM IM is below 200 mesh, the reaction is ...

Embodiment 3

[0039] The preparation of embodiment 3 biological pesticides

[0040] Example 3 The biopesticide containing fatty acid glycerides of residual rice dregs comprises the following components in parts by weight: 20 parts of fatty acid glycerides of rice dregs residual oil, 35 parts of Bacillus soree, 64 parts of hydroxyapatite, and 16 parts of white carbon black , 20 parts of starch and an appropriate amount of water.

[0041] Preparation method: Mix fatty acid glycerides of rice dregs residual oil, Bacillus suyunjin, hydroxyapatite, white carbon black, starch and water, stir evenly, carry out wet granulation, make granules with a diameter of 0.2-0.4cm, and vacuum Drying until the water content is 5-10%wt, the biopesticide can be obtained.

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Abstract

The invention discloses bio-pesticide containing rice dreg residual oil glycerin fatty acid ester and a preparation method thereof. The bio-pesticide comprises the following components in parts by weight: 15 to 25 parts of the rice dreg residual oil glycerin fatty acid ester, 20 to 35 parts of bacillus thuringiensis, 80 to 100 parts of filler, 10 to 15 parts of a binding agent and a proper amountof water. The bio-pesticide disclosed by the invention has the advantages of wide insecticidal spectrum, high insecticidal activity, rapid and stable insecticidal effect, long residual effect period,good advanced-age larva killing effect, high efficiency, low toxicity, low residues and environment friendliness. Meanwhile, cyclic utilization of rice dreg waste oil can be realized and an energy-saving and environment-protection concept is met; and wider application of the bacillus thuringiensis can be promoted.

Description

technical field [0001] The invention belongs to the technical field of biopesticide preparation, and in particular relates to a biopesticide containing fatty acid glyceride of rice dregs and a preparation method thereof. Background technique [0002] Biopesticide refers to a type of pesticide preparation that uses living organisms or their metabolites to control pests, germs, weeds, nematodes, rodents and other harmful organisms. Biological pesticides include microbial-derived pesticides, plant-derived pesticides, animal-derived pesticides and genetically modified Compared with chemical pesticides, biological pesticides have the following advantages: 1) strong selectivity, relatively safe for humans, animals and various beneficial organisms, and protect natural enemies; 2) have little impact on the ecological environment; 3) can induce pests Epidemics etc. [0003] Microbial pesticides are an important part of biopesticides. They are made from microbial groups whose metabol...

Claims

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Application Information

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IPC IPC(8): A01N63/00A01N37/00A01P7/00C12P7/62
CPCA01N37/00A01N63/00C12P7/62
Inventor 何美英
Owner 上海沪联生物药业(夏邑)股份有限公司
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